Shinwa Chemical Industries Ltd.
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Shinwa Chemical Industries
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"GLY" Filtered 35 Item.

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GC

Samples
Trimethylamine , Dimethylamine , Monomethylamine
Applications
Mono-, di-, trimethylamine
Column
Diglycerol+TEP+KOH(15%+15%+2%) Chromosorb W 80-100 (AW-DMIS)
Column Size
3.1m×3.2mm
Column temp.
70°C
Carrier gas
N2,60ml/min
Injection port temp.
230°C
Detector temp.
230°C(FID)

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GC

Samples
Ethyleneglycol , Diethyleneglycol , Triethyleneglycol
Applications
Glycols (1)
Column
TENAX TA 60-80
Column Size
1.1m×3.2mm
Column temp.
180°C→210°C(3°C/min)
Carrier gas
N2,50ml/min
Injection port temp.
260°C
Detector temp.
260°C(FID)

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GC

Samples
Propyleneglycol , Ethyleneglycol , Decyl Alcohol , 1,4-Butanediol , Diethyleneglycol , Lauryl Alcohol , Myristyl Alcohol , Triethyleneglycol , Cetyl Alcohol , Stearyl Alcohol
Applications
Glycol and higher alcohol
Column
Thermon-3000 1% Shimalite TPA 60-80
Column Size
1.1m×3.2mm
Column temp.
90°C→180°C(5°C/min)
Carrier gas
N2,60ml/min
Injection port temp.
260°C
Detector temp.
260°C(FID)

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GC

Samples
Triglyceride
Applications
The oil ball
Column
ULBON HR-TGC1
Column Size
25m×0.25mm(0.1μm)
Column temp.
100°C→390°C(8°C/min)
Carrier gas
He,1.5kg/cm2
Detector temp.
390°C(FID)
Injection volume
1μl

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GC

Samples
Triglyceride
Applications
Calnaubawax
Column
ULBON HR-TGC1
Column Size
25m×0.25mm(0.1μm)
Column temp.
250°C→380°C(5°C/min)
Carrier gas
He,1.3kg/cm2
Detector temp.
390°C(FID)
Injection volume
0.2μl

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GC

Samples
Triglyceride
Applications
Triglyceride
Column
ULBON HR-TGC1
Column Size
25m×0.25mm(0.1μm)
Column temp.
250°C→380°C(5°C/min)
Carrier gas
He,1.3kg/cm2
Detector temp.
390°C(FID)
Injection volume
0.2μl

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GC

Samples
Trimethylamine , Dimethylamine , Methylamine
Applications
Analysis of methylamines using Shinwasorb
Column
Diglycerol+TEP+KOH 7.5+7.5+1% Shinwasorb-S 60/80
Column Size
3.1 m x 3.2 mm I.D. Glass
Column temp.
70℃
Carrier gas
50 mL/min N₂
Injection port temp.
220℃
Detector temp.
220℃
Detector
FID
Injection volume
1.0 μL

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GC

Samples
Mixture of 22 organic solvents
Applications
Measurement of organic solvents using Shinwasorb -2-
Column
PEG1500 12.5% Shinwasorb-U 40/60
Column Size
2.1 m x 3.2 mm I.D. Glass
Column temp.
60~120℃ (4℃/min)
Carrier gas
40 mL/min N₂
Injection port temp.
200℃
Detector temp.
200℃
Detector
FID
Injection volume
1.0 μL

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GC

Samples
Propyleneglycol , 1,3-propanediol
Applications
Measurement of food additives using Sunpak-A
Column
Sunpak-A 50/80
Column Size
2.1 m x 3.2 mm I.D. Glass
Column temp.
180℃
Carrier gas
50 mL/min N₂
Injection port temp.
200℃
Detector temp.
230℃
Detector
FID
Injection volume
1.0 μL

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GC

Samples
Propyleneglycol , 1,3-propanediol
Applications
Measurement of food additives using Sunpak-A
Column
Sunpak-A 50/80
Column Size
2.1 m x 3.2 mm I.D. Glass
Column temp.
180℃
Carrier gas
50 mL/min N₂
Injection port temp.
200℃
Detector temp.
230℃
Detector
FID
Injection volume
1.0 μL

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GC

Samples
Ethylene glycol , Diethylene glycol
Applications
Analysis of macrogol 400 using Shinwasorb
Column
Sorbitol 3% Shinwasorb-S 80/100
Column Size
1.6 m x 3.2 mm I.D. Glass
Column temp.
160℃
Carrier gas
47 mL/min N2
Injection port temp.
200°C
Detector temp.
200°C
Detector
FID
Injection volume
2.0 μL

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GC

Samples
Acetone , Allethrin , Di(2-ethylhexyl) phthalate
Applications
Analysis of allethrin using Shinwasorb Part 3
Column
Diethyleneglycol Succinate (DEGS) 2.5% Shinwasorb-U 80/100
Column Size
1.1 m x 3.2 mm I.D. Glass
Column temp.
200℃
Carrier gas
36 mL/min N₂ (Adjust so that the retention time of allethrin is about 8 minutes.)
Injection port temp.
230°C
Detector temp.
230°C
Detector
FID
Injection volume
1.0 μL

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LC

Samples
Chlorphenesin
Applications
Muscle relaxant
Column
ULTRON ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20mM KH2PO4 (pH 5.5)
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Chlorphenesin
Applications
Muscle relaxant
Column
ULTRON ES-PhCD
Column Size
150 mm L × 6.0 mm I.D.
Mobile phase
20 mM KH2PO4 (pH 4.6)/CH3CN = 70/30
Frow rate
0.6 mL/min
Column temp.
9°C

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LC

Samples
Ethylene glycol , Diethylene glycol , Methanol , Ethanol , Isopropyl alcohol
Applications
Alcohols
Column
ULTRON PS-80H
Column Size
300 mm L × 8.0 mm I.D.
Mobile phase
H2O
Frow rate
1.0 mL/min
Column temp.
60°C
Pressure
2.5 MPa
Injection volume
6.0 µL (10 mg/mL)

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LC

Samples
Citric acid , Tartaric acid , Malic acid , Malonic acid , Succinic acid , Glycolic acid , Formic acid , Lactic acid , Acetic acid , Fumaric acid , Adipic acid , Pyroglutamic acid , Propionic acid , Acrylic acid , Pivalic acid , Methacrylic acid , Crotonic acid
Applications
Elution position of the aliphatic organic acid
Column
ULTRON PS-80H
Column Size
300 mm L × 8.0 mm I.D. + 300 mm L × 8.0 mm I.D.
Mobile phase
HClO4aq. (pH 2.1)
Frow rate
1.0 mL/min
Column temp.
60°C

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LC

Samples
Maltotriose , Maltose , Glucose , Glycerol , Ethanol
Applications
Sake
Column
ULTRON PS-80N
Column Size
300 mm L × 8.0 mm I.D.
Mobile phase
H2O
Frow rate
1.0 mL/min
Column temp.
60°C
Pressure
2.2 MPa
Injection volume
10 µL (undiluted solution)

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LC

Samples
Aspartic acid , Glutamic acid , Serine , Glycine , Histidine , Arginine , Threonine , Alanine , Proline , Tyrosine , Valine , Methionine , Cysteine-cysteine , Isoleucine , Leucine , Phenylalanine , Lysine
Applications
Analysis of the PTC amino acid
Column
STR ODS-II
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
A: CH3COONa (pH 6.5)/CH3CN = 93/7, B: CH3CN/H2O = 4/1
Frow rate
1.0 mL/min
Column temp.
40°C

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LC

Samples
Iprodione, Bensulide
Applications
Iprodione, Bensulide
Column
STR ODS-II
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
CH3CN/H2O = 60/40
Frow rate
1.0 mL/min
Column temp.
40°C

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LC

Samples
Hippuric acid , o-Methyl hippuric acid , p-Methyl hippuric acid , m-Methyl hippuric acid
Applications
Hippuric acid
Column
STR ODS-II
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM Phosphoric acid buffer (pH 2.5) + 10 mM β-Cyclodextrin/CH3CN = 8/1
Frow rate
1.0 mL/min
Column temp.
50°C

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LC

Samples
Glycyrrhetic acid , Propyl paraben
Applications
Glycyrrhizin in the licorice end
Column
STR ODS-II
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
15 times dilution Acetic acid aqueous solution/CH3CN = 3/2
Frow rate
0.7 mL/min
Column temp.
ambient

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LC

Samples
Cholic acid , Glycocholic acid , Taurocholic acid , Chenodeoxycholic acid , Glycochenodeoxycholic acid , Deoxycholic acid , Taurochenodeoxycholic acid , Taurodeoxycholic acid
Applications
Bile acid
Column
STR ODS-II
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
CH3CN/30 mM (NH4)2HPO4(Ajusted to pH 7.2 with NH4H2PO4), A: 10/90, B: 50/50
Frow rate
1.0 mL/min
Column temp.
40°C

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LC

Samples
Glycyrrhizin
Applications
Glycyrrhizin
Column
ULTRON VX-ODS
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4(pH 4.6)/CH3CN = 7/3
Frow rate
1.0 mL/min
Column temp.
30°C

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LC

Samples
Glycyrrhetic acid
Applications
Glycyrrhetic acid
Column
ULTRON VX-ODS
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4(pH 4.6)/CH3CN = 1/4
Frow rate
1.0 mL/min
Column temp.
30°C

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LC

Samples
Allantoin , Xanthine , Hypoxanthine , Uric acid
Applications
Uric acid metabolites
Column
ULTRON AF-HILIC-CD
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
10 mM CH3CO2NH4(pH 4.7)/CH3CN = 10/90
Frow rate
0.35 mL/min
Column temp.
30°C
Injection volume
1.0 µL

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LC

Samples
Urea , Xanthine , Lactic acid , Creatinine , Uric acid
Applications
Sweat Composition
Column
ULTRON AF-HILIC-CD (PLSS)
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
10 mM HCO2NH4(pH 3.0)/CH3CN = 10/90
Frow rate
0.30 mL/min
Column temp.
30°C
Injection volume
1.0 µL

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LC

Samples
(CYS)2 , LYS , ARG , HIS , ASP , GLU , GLN , ASN , GLY , SER , ALA , THR , PRO , TYR , VAL , PHE , MET , TRP , LEU+ILE
Applications
Analysis of underivatized amino acids by LC/MS/MS
Column
ULTRON AF-HILIC-CD (PLSS)
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
A: 100 mM HCO2NH4(pH 3.0)/CH3CN = 10/90, B: 100 mM HCO2NH4(pH 3.0)/CH3CN = 70/30
Frow rate
0.36 mL/min
Column temp.
40°C
Injection volume
1.0 µL (5.0 µg/mL)

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LC

Samples
Fucose , Xylose , GalNAc , Mannose , Glucose , GluNAc , Galactose , Neu5Ac , Glucuronic acid
Applications
Glycan-constituting monosaccharides
Column
ULTRON AF-HILIC-CD
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
A: 200 mM CH3CO2NH4(pH 6.8)/CH3CN = 10/90 (for peak 1 to 7), B: 200 mM CH3CO2NH4(pH 6.8)/CH3CN = 18/82 (for peak 8 and 9)
Frow rate
0.26 mL/min
Column temp.
45°C
Injection volume
1.0 µL

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LC

Samples
1-Methylpyrazole , Fomepizole , Pyrazole , 1H-1,2,3-Triazole , Pyrazoline , Imidazole ,
Applications
Analysis of heterocyclic compounds
Column
ULTRON AF-HILIC-DA
Column Size
100 mm L × 4.6 mm I.D.
Mobile phase
20mM HCO2NH4 (pH3.2) /CH3CN = 10/90
Frow rate
0.50 mL/min
Column temp.
30°C
Injection volume
4.0 µL
Diluent
mobile phase

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LC

Samples
Maleic acid , Pyruvic acid , Ascorbic acid , Gluconic acid , Adipic acid , Fumaric acid , Tartaric acid , Malic acid , Citric acid
Applications
Analysis of organic acid
Column
ULTRON AF-HILIC-CD (PLSS)
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
100mM CH3CO2NH4 (pH6.8) /CH3CN = 25/75
Frow rate
0.20 mL/min
Column temp.
40°C
Injection volume
2.0 µL
Diluent
mobile phase

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LC

Samples
Allantoin , Xanthine , Hypoxanthine , Uric acid
Applications
Analysis of Uric acid metabolite
Column
ULTRON AF-HILIC-CD
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
10mM CH3CO2NH4 (pH4.7) /CH3CN = 10/90
Frow rate
0.35 mL/min
Column temp.
30°C
Injection volume
1.0 µL
Diluent
Dissolved samples in 0.1% NaOH aq and add acetonitrile into ratio to 50%

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LC

Samples
Turanose , Palatinose , Maltulose , Maltose , Lactose , Trehalose
Applications
Analysis of disaccharides with different glycosidic linkages
Column
ULTRON AF-HILIC-CD
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
100mM CH3CO2NH4 (pH6.8) /CH3CN = 10/90
Frow rate
0.45 mL/min
Column temp.
40°C
Injection volume
1.0 µL
Diluent
H2O /CH3CN = 50/50

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LC

Samples
Val-Tyr-Val , Leucine Enkephalin , Methionine Enkephalin , Gly-Tyr
Applications
Analysis of peptide standards
Column
ULTRON AF-HILIC-CD
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
A: 10mM HCO2NH4 (pH3.0) /CH3CN = 10/90, B: 10mM HCO2NH4 (pH3.0) /CH3CN = 70/30
Frow rate
0.26 mL/min: 67% A/ 33% B (70.0% CH3CN)
Column temp.
40°C
Injection volume
2.0 µL
Diluent
H2O /CH3CN = 50/50

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LC

Samples
Glycopyrronium bromide
Applications
Analysis of Glycopyrronium bromide
Column
ULTRON ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4 + 20mM K2HPO4 (pH 5.5)/C2H5OH = 95/5
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
2.0 µL

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LC

Samples
Glycopyrrolate , Glycopyrrolate erythro isomer
Applications
Analysis of Glycopyrrolate
Column
ULTRON ES-CD
Column Size
250 mm L × 4.6 mm I.D.
Mobile phase
23.3 mM NaH2PO4(pH 6.5)/CH3OH/CH3CN = 40/50/10
Frow rate
1.0 mL/min
Column temp.
30°C
Injection volume
10.0 µL
Diluent
mobile phase

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