GC

Samples

Trimethylamine , Dimethylamine , Monomethylamine

Applications

Mono-, di-, trimethylamine

Column

Diglycerol+TEP+KOH(15%+15%+2%) Chromosorb W 80-100 (AW-DMIS)

Column Size

3.1m×3.2mm

Column temp.

70°C

Carrier gas

N2,60ml/min

Injection port temp.

230°C

Detector temp.

230°C(FID)

View detail

GC

Samples

Mono Ethanolamine , Diethanolamine , Triethanolamine

Applications

Tri-, di-, monoethanolamine in water

Column

TENAX TA 60-80

Column Size

1.1m×3.2mm

Column temp.

160°C→270°C(10°C/min)

Carrier gas

N2,40ml/min

Injection port temp.

290°C

Detector temp.

290°C(FID)

View detail

GC

Samples

TETA(Triethylene Tetramine) , TEPA(Tetraethylene Pentamine)

Applications

TETA and TEPA

Column

Thermon-1000+KOH(10%+3%) Chromosorb W 80-100 (AW-DMCS)

Column Size

2.1m×3.2mm

Column temp.

250°C

Carrier gas

N2,55ml/min

Injection port temp.

280°C

Detector temp.

280°C(FID)

View detail

GC

Samples

o-Phenylenediamine , p-Phenylenediamine , m-Phenylenediamine

Applications

Phenylenediamine

Column

Thermon-1000+KOH(10%+3%) Chromosorb W 80-100 (AW-DMCS)

Column Size

2.1m×3.2mm

Column temp.

250°C

Carrier gas

N2,60ml/min

Injection port temp.

280°C

Detector temp.

280°C(FID)

View detail

GC

Samples

Diphenhydramine

Applications

Diphenhydramine

Column

Thermon-3000 5% Chromosorb W 80-100 (AW-DMCS)

Column Size

1.1m×3.2mm

Column temp.

200°C

Carrier gas

N2,80ml/min

Injection port temp.

260°C

Detector temp.

260°C(FID)

View detail

GC

Samples

Monomethylamine , Dimethylamine , Trimethylamine

Applications

Tri-, di-, monomethylamine in Nitrogen

Column

Thermon-3000+KOH(5%+1%) Sunpak-A

Column Size

2.1m×3.2mm

Column temp.

150°C

Carrier gas

N2,50ml/min

Injection port temp.

240°C

Detector temp.

240°C(FID)

View detail

GC

Samples

Methylamine , Dimethylamine , Trimethylamine

Applications

Tri-, di-, monomethylamine in water

Column

Thermon-3000+KOH(5%+1%) Sunpak-A

Column Size

2.1m×3.2mm

Column temp.

140°C

Carrier gas

N2,50ml/min

Injection port temp.

250°C

Detector temp.

230°C(FID)

View detail

GC

Samples

Methanol , Acetaldehyde , Ethanol , Trimethylamine

Applications

Methanol Ethanol Acetaldehyde Trimethylamine in water

Column

Thermon-3000+KOH(5%+1%) Sunpak-A

Column Size

2.1m×3.2mm

Column temp.

120°C

Carrier gas

N2,50ml/min(headspace)

Injection port temp.

220°C

Detector temp.

220°C(FID)

View detail

GC

Samples

Monomethylamine , Dimethylamine , Trimethylamine

Applications

Tri-, di-, monomethylamine in water

Column

Thermon-3000+KOH(5%+1%) Sunpak-A

Column Size

2.1m×3.2mm

Column temp.

140°C

Carrier gas

N2,50ml/min

Injection port temp.

260°C

Detector temp.

260°C(FID)

View detail

GC

Samples

o-Ethoxybenzamide , Phenacetin , Caffeine , Aminopyrine , Chlorpheniramine Maleate

Applications

Medicine

Column

ULBON HR-1

Column Size

15m×0.53mm(1.0μm)

Column temp.

180°C

Carrier gas

He,7.2ml/min

Detector temp.

250°C(FID)

Injection volume

0.5μl

View detail

GC

Samples

n-Octylamine , n-Decylamine , Laurylamine , n-Tetradecylamine , Cetylamine , Stearylamine

Applications

Aliphatic amine

Column

ULBON HR-52

Column Size

25m×0.25mm(0.25μm)

Column temp.

150°C→230°C(4°C/min)

Carrier gas

He,0.48ml/min

Detector temp.

250°C(FID)

Injection volume

1.5μl

View detail

GC

Samples

Trimethylamine , Dimethylamine , Methylamine

Applications

Analysis of methylamines using Shinwasorb

Column

Diglycerol+TEP+KOH 7.5+7.5+1% Shinwasorb-S 60/80

Column Size

3.1 m x 3.2 mm I.D. Glass

Column temp.

70℃

Carrier gas

50 mL/min N₂

Injection port temp.

220℃

Detector temp.

220℃

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

homatropine hydrobromide , scopolamine

Applications

Analysis of opium alkaloid scopolamine using Shinwasorb

Column

Silicone OV-17 1% Shinwasorb-S 60/80

Column Size

1.6m×3.2mm glass

Column temp.

210°C

Carrier gas

45 mL/min N2

Injection port temp.

250°C

Detector temp.

250°C

Detector

FID

Injection volume

2.0 μL

View detail

GC

Samples

Ammonia and Mono, Di, Tri-Methylamine in Water ,

Applications

Ammonia and Mono, Di, Tri-Methylamine in Water

Column

Thermon-3000 + KOH 2+2% Sunpak-N 60/100 mesh

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

120℃

Carrier gas

50 mL/min He

Injection port temp.

250°C

Detector temp.

250°C

Detector

TCD

Injection volume

1.0 μL

View detail

LC

Samples

Alimemazine

Applications

Antihistaminic drug

Column

ULTRON ES-CD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 5.0)/CH3CN = 70/30

Frow rate

1.2 mL/min

Column temp.

25°C

View detail

LC

Samples

Trimipramine

Applications

Trimipramine

Column

ULTRON ES-CD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 4.6)/CH3CN = 75/25

Frow rate

1.2 mL/min

Column temp.

25°C

View detail

LC

Samples

Chlorpheniramine maleate

Applications

Chlorpheniramine maleate

Column

ULTRON ES-CD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 4.6)/CH3CN = 83/17

Frow rate

1.0 mL/min

Column temp.

15°C

View detail

LC

Samples

1,2-Diphenylethylamine

Applications

1,2-Diphenylethylamine

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 5.5)

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Prenylamine

Applications

Calcium rivalry medicine

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 5.0)/CH3CN = 100/15

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Trimipramine maleate

Applications

Analysis of the antidepressive drug

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 3.0)/C2H5OH = 100/30

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Profenamine

Applications

Antiparkinsonic agent

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 4.6)/C2H5OH = 100/25

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Alimemazine

Applications

Antihistaminic drug

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 4.6)/C2H5OH = 100/25

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Chlorpheniramine

Applications

Antihistaminic drug

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 5.0)/CH3CN = 100/5

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Dimethindene maleate

Applications

Antihistaminic drug

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 4.6)/CH3CN = 100/9

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Promethazine

Applications

Antihistaminic drug

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 3.0)/CH3CN = 100/5

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

α-Phenylethylamine , (S)-(-)-α-Methylbenzylamine

Applications

α-Phenylethylamine

Column

ULTRON ES-PhCD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 4.6)/CH3CN = 95/5

Frow rate

0.6 mL/min

Column temp.

15°C

View detail

LC

Samples

N-(3,5-Dinitrobenzoyl)-α-Methylbenzylamine

Applications

Analysis in normal phase mobile phase

Column

ULTRON ES-PhCD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

n-Hexane/C2H5OH = 85/15

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Bunitrolol

Applications

β-Blocking agent

Column

ULTRON ES-PhCD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 4.6)/CH3CN = 70/30

Frow rate

1.2 mL/min

Column temp.

25°C

View detail

LC

Samples

Glucuronic acid , N-Acetylglucosamine , N-Acetylgalactosamine

Applications

Uronic acid, Acetylation amino sugar

Column

ULTRON PS-80H

Column Size

300 mm L × 8.0 mm I.D.

Mobile phase

HClO4aq. (pH 2.1)

Frow rate

1.0 mL/min

Column temp.

60°C

Pressure

2.5 MPa

View detail

LC

Samples

Cytosine , Uracil , Guanine , Adenine , Cytidine , Uridine , Thymine , Adenosine , Guanosine , Thymidine

Applications

Nucleic acid base, Nucleoside

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

0.1 M Phosphoric acid buffer (pH 2.1) + 0.2 M NaClO4

Frow rate

1.0 mL/min

Column temp.

50°C

View detail

LC

Samples

Methylephedrine hydrochloride , Noscapine , Thiamine , Dextromethorphan , Carbinoxamine maleate

Applications

The component of the cold remedy (1)

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

CH3CN/H2O/H3PO4 = 510/490/1 + 0.5% Sodium dodecyl sulfate

Frow rate

1.0 mL/min

Column temp.

50°C

View detail

LC

Samples

Salicylic acid , Diphenhydramine , Methyl salicylate , α-Camphor , Thymol

Applications

The component of the anti-inflammatory agent

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

10 mM Phosphoric acid buffer(pH 2.6) + 20 mM Heptane sodium sulphonate/CH3OH/CH3CN = 3/2/2

Frow rate

1.0 mL/min

Column temp.

45°C

View detail

LC

Samples

Nicotinic acid , Nicotinamide , Pantothenic acid , Pyridoxine , Riboflavin phosphate , Thiamine , Caffeine , Folic acid , Biotin , Riboflavin

Applications

The water-soluble vitamin (1)

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

100 mM Phosphoric acid buffer(pH 2.1) + 0.8 mM Octane sodium sulphonate/CH3CN = 9/1

Frow rate

1.0 mL/min

Column temp.

40°C

View detail

LC

Samples

Pyridoxal , Pyridoxine , Pyridoxamine

Applications

The water-soluble vitamin (2)

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

100 mM Phosphoric acid buffer(pH 2.1) + 50 mM Hexane sodium sulphonate/CH3CN = 9/1

Frow rate

1.0 mL/min

Column temp.

45°C

View detail

LC

Samples

Nicotinic acid , Nicotinic acid amide , Calcium pantothenate , Pyridoxine hydrochloride , Riboflavin phosphate , Thiamine , Folic acid , Biotin , Riboflavin

Applications

The water-soluble vitamin

Column

ULTRON VX-ODS

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM H3PO4/5 mM Sodium 1-hexanesulfonate = 91/9

Frow rate

1.0 mL/min

Column temp.

45°C

View detail

LC

Samples

Bepotastine besilate

Applications

Bepotastine besilate

Column

ULTRON ES-CD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

20 mM KH2PO4(pH 4.6)/CH3CN = 75/25

Frow rate

0.7 mL/min

Column temp.

40°C

View detail

LC

Samples

Bepotastine besilate

Applications

Bepotastine besilate

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4(pH 4.6)/CH3CN = 90/10

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Brompheniramine maleate

Applications

Brompheniramine maleate

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4(pH 4.6)/CH3CN = 90/10

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Bupropion hydrochloride

Applications

Bupropion hydrochloride

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + 20 mM K2HPO4(pH 6.0)/C2H5OH = 90/10

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Cetirizine hydrochloride

Applications

Cetirizine hydrochloride

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + 20 mM K2HPO4(pH 6.0)/CH3CN = 90/10

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2 µL

Diluent

mobile phase

View detail

LC

Samples

Cetirizine hydrochloride

Applications

Cetirizine hydrochloride

Column

ULTRON ES-OVM

Column Size

100 mm L × 3.0 mm I.D.

Mobile phase

20 mM KH2PO4 + 20 mM K2HPO4(pH 6.0)/CH3CN = 90/10

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Doxylamine succinate

Applications

Doxylamine succinate

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + 20 mM K2HPO4(pH 6.0)/CH3CN = 90/10

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Nicotinamide , Pyridoxine , Isoascorbic acid , Riboflavin , Nicotinic acid , Ascorbic acid , Biotin , Pantothenic acid , Folic acid , Cyanocobalamin , Thiamine

Applications

Water-soluble vitamins

Column

ULTRON AF-HILIC-CD

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

A: 20 mM CH3CO2NH4(pH 6.8)/CH3CN = 10/90, B: 20 mM CH3CO2NH4(pH 6.8)/CH3CN = 70/30

Frow rate

0.25 mL/min

Column temp.

30°C

Injection volume

1.0 µL

View detail

LC

Samples

(CYS)2 , LYS , ARG , HIS , ASP , GLU , GLN , ASN , GLY , SER , ALA , THR , PRO , TYR , VAL , PHE , MET , TRP , LEU+ILE

Applications

Analysis of underivatized amino acids by LC/MS/MS

Column

ULTRON AF-HILIC-CD (PLSS)

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

A: 100 mM HCO2NH4(pH 3.0)/CH3CN = 10/90, B: 100 mM HCO2NH4(pH 3.0)/CH3CN = 70/30

Frow rate

0.36 mL/min

Column temp.

40°C

Injection volume

1.0 µL (5.0 µg/mL)

View detail

LC

Samples

Fucose , Xylose , GalNAc , Mannose , Glucose , GluNAc , Galactose , Neu5Ac , Glucuronic acid

Applications

Glycan-constituting monosaccharides

Column

ULTRON AF-HILIC-CD

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

A: 200 mM CH3CO2NH4(pH 6.8)/CH3CN = 10/90 (for peak 1 to 7), B: 200 mM CH3CO2NH4(pH 6.8)/CH3CN = 18/82 (for peak 8 and 9)

Frow rate

0.26 mL/min

Column temp.

45°C

Injection volume

1.0 µL

View detail

LC

Samples

Cyanuric acid , Ammelide , Melamine , Ammeline

Applications

Melamine-related compounds

Column

ULTRON AF-HILIC-CD

Column Size

100 mm L × 2.0 mm I.D.

Mobile phase

20 mM HCO2NH4(pH 6.8)/CH3CN = 18/82

Frow rate

0.15 mL/min

Column temp.

30°C

Injection volume

0.8 µL

View detail

LC

Samples

L-DOPA , Dopamine , Adrenaline , Noradrenaline

Applications

Analysis of catecholamines

Column

ULTRON AF-HILIC-DA

Column Size

100 mm L × 4.6 mm I.D.

Mobile phase

20mM CH3CO2NH4 (pH4.7) /CH3CN = 10/90

Frow rate

0.50 mL/min

Column temp.

30°C

Injection volume

4.0 µL

Diluent

mobile phase

View detail

LC

Samples

Cyanuric acid , Ammelide , Melamine , Ammeline

Applications

Analysis of melamine compounds

Column

ULTRON AF-HILIC-CD

Column Size

100 mm L × 2.0 mm I.D.

Mobile phase

20mM HCO2NH4 (pH6.8) /CH3CN = 18/82

Frow rate

0.15 mL/min

Column temp.

30°C

Injection volume

2.0 µL

Diluent

Dissolved samples in 0.1% NaOH aq and add acetonitrile into ratio to 50%

View detail

LC

Samples

Atomoxetine hydrochloride

Applications

Analyses of Atomoxetine hydrochloride in ULTRON ES-OVM series.(Faster analyses with 3µm particles)

Column

ULTRON ES-OVM

Column Size

(1)150 mm L × 4.6 mm I.D.　(2)100 mm L × 3.0 mm I.D.

Mobile phase

20 mM KH2PO4 + 20 mM K2HPO4 (pH 6.0)/CH3CN = 80/20

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

(1)2.0 µL (2)0.5 µL

Diluent

methanol

View detail

LC

Samples

Duloxetine hydrochloride

Applications

Analyses of Duloxetine hydrochloride in ULTRON ES-OVM series.(Faster analyses with 3µm particles)

Column

ULTRON ES-OVM

Column Size

(1)150 mm L × 4.6 mm I.D.　(2)100 mm L × 3.0 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 4.6)/CH3CN = 80/20

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

(1)2.0 µL (2)0.5 µL

Diluent

mobile phase

View detail

LC

Samples

Atomoxetine hydrochloride

Applications

Analyses of Atomoxetine hydrochloride in ULTRON ES-OVM series.(Greater analytical performance with 3µm particles)

Column

ULTRON ES-OVM

Column Size

(1)150 mm L × 4.6 mm I.D.　(2)100 mm L × 3.0 mm I.D.

Mobile phase

20 mM KH2PO4 + 20 mM K2HPO4 (pH 6.0)/CH3CN = 80/20

Frow rate

(1)1.0 mL/min　(2)0.28 mL/min

Column temp.

25°C

Injection volume

(1)2.0 µL　(2)0.5 µL

Diluent

methanol

View detail

LC

Samples

Duloxetine hydrochloride

Applications

Analyses of Duloxetine hydrochloride in ULTRON ES-OVM series.(Greater analytical performance with 3µm particles)

Column

ULTRON ES-OVM

Column Size

(1)150 mm L × 4.6 mm I.D.　(2)100 mm L × 3.0 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 4.6)/CH3CN = 80/20

Frow rate

(1)1.0 mL/min　(2)0.28 mL/min

Column temp.

25°C

Injection volume

(1)2.0 µL　(2)0.5 µL

Diluent

mobile phase

View detail

LC

Samples

Sertraline hydrochloride

Applications

Analysis of Sertraline hydrochloride

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

Diluent

methanol

View detail

LC

Samples

Sertraline hydrochloride

Applications

Analysis of Sertraline hydrochloride

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

Diluent

methanol

View detail

LC

Samples

Cinacalcet hydrochloride

Applications

Analysis of Cinacalcet hydrochloride

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 93/7

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

Diluent

ethanol

View detail

LC

Samples

Sertraline hydrochloride , Sertraline Hydrochloride Related Compound A

Applications

Analysis of Sertraline hydrochloride

Column

ULTRON ES-CD

Column Size

250 mm L × 4.6 mm I.D.

Mobile phase

50.4mM NH4H2PO4 (pH 4.2)/CH3OH = 52/48

Frow rate

1.0 mL/min

Column temp.

30°C

Injection volume

20.0 µL

Diluent

mobile phase

View detail

LC

Samples

Atomoxetine hydrochloride

Applications

Analysis of Atomoxetine hydrochloride

Column

ULTRON ES-OVM

Column Size

100 mm L × 3.0 mm I.D.

Mobile phase

20 mM KH2PO4 + 20 mM K2HPO4 (pH 6.0)/CH3CN = 80/20

Frow rate

0.28 mL/min

Column temp.

25°C

Injection volume

0.5 µL

Diluent

methanol

View detail

LC

Samples

Duloxetine hydrochloride

Applications

Analysis of Duloxetine hydrochloride

Column

ULTRON ES-OVM

Column Size

100 mm L × 3.0 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 4.6)/CH3CN = 80/20

Frow rate

0.28 mL/min

Column temp.

25°C

Injection volume

0.5 µL

Diluent

mobile phase

View detail