GC

Samples

Methyl iodide , iso-Propyl iodide , n-Octane , o-Xylene

Applications

Analysis of hypromellose using Shinwasorb

Column

Silicone DC-200 10% Shinwasorb-S 100/120

Column Size

3.1 m x 3.2 mm I.D. Glass

Column temp.

90℃

Carrier gas

38 mL/min N₂

Injection port temp.

200℃

Detector temp.

200℃

Detector

FID

Injection volume

2.0 μL

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GC

Samples

Carbon sulfide , Hydrogen sulfide , Carbon disulfide , Methyl mercaptan , Ethyl mercaptane , Dimethyl sulfide

Applications

Measurements of offensive odor substances using Shinwasorb -3-

Column

1,2,3-TCEP 25% Shinwasorb-S 80/100 ST

Column Size

3.1 m x 3.2 mm I.D. Glass

Column temp.

70℃

Carrier gas

50 mL/min N₂

Injection port temp.

180℃

Detector temp.

180℃

Detector

FPD

Injection volume

1.0 μL

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GC

Samples

Chloroform , Ethanol , Naphthalene , Amantadine

Applications

Measurements of amantadine hydrochloride using Shinwasorb

Column

Apiezone L+KOH 2+1% Shinwasorb-S 80/100

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

125℃(5 min hold)～150℃(5℃/min)～150℃ (10 min hold)

Carrier gas

50 mL/min N₂

Injection port temp.

200℃

Detector temp.

200℃

Detector

FID

Injection volume

2.0 μL

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GC

Samples

200 ppm in hexane

Applications

Measurements of eucalyptus oil using Shinwasorb

Column

Thermon-3000 5% Shinwasorb-S 80/100

Column Size

5.1 m x 3.2 mm I.D. Glass

Column temp.

120℃ & 130℃

Carrier gas

40 mL/min N₂

Injection port temp.

200℃

Detector temp.

200℃

Detector

FID

Injection volume

2.0 μL

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GC

Samples

Isopropyl iodide , Methylcyclohexane , o-xylene

Applications

Analysis of hydroxypropylcellulose (JP)

Column

ULBON HR-1

Column Size

0.53 mm I.D. x 30 m df = 3.0 µm

Column temp.

40℃ (3 min)～10℃/min～100℃～50℃/min～250℃ (3 min)

Carrier gas

52 cm/sec He

Injection port temp.

180°C

Detector temp.

280°C

Detector

FID

Injection volume

2.0 μL Split rate: 1:50

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GC

Samples

Ethylene glycol , Diethylene glycol

Applications

Analysis of macrogol 400 using Shinwasorb

Column

Sorbitol 3% Shinwasorb-S 80/100

Column Size

1.6 m x 3.2 mm I.D. Glass

Column temp.

160℃

Carrier gas

47 mL/min N2

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

2.0 μL

View detail

GC

Samples

Cyclohexane , N,N-dimethylaniline , Naphthalene ,

Applications

Analysis of ampicillin hydrate using Shinwasorb

Column

Silicone OV-17 1.5% Shinwasorb-S 60/80

Column Size

2.1 m x 2.6 mm I.D. Glass

Column temp.

105℃

Carrier gas

20 mL/min He（adjust so that the retention time of N,N-dimethylaniline is about 5 minutes.)

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

Cyclohexane , Ethyl acetate , 2-propanol ,

Applications

Analysis of lenampicillin hydrochloride using Shinwasorb

Column

Quadrol 5% Shinwasorb-S 60/80

Column Size

3.1 m x 3.2 mm I.D. Glass

Column temp.

100℃

Carrier gas

70 mL/min N₂ (Adjust so that the retention time of cyclohexane is about 1 minute.)

Injection port temp.

160°C

Detector temp.

160°C

Detector

FID

Injection volume

4.0 μL

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GC

Samples

Enflurane , 2-propanol ,

Applications

Analysis of enflurane using Shinwasorb

Column

DEGS 10% Shinwasorb-S 60/80

Column Size

3.1 m x 3.2 mm I.D. Glass

Column temp.

80℃

Carrier gas

32 mL/min He (Adjust so that the retention time of enflurane is about 3 minutes.)

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

5.0 μL

View detail

GC

Samples

Isoflurane , Ethyl acetate

Applications

Analysis of isoflurane using Shinwasorb

Column

Igepal CO-880+Ucon LB-550X 5+7.5% Shinwasorb-S 100/120

Column Size

3.5 m x 3.0 mm I.D. Stainless steel

Column temp.

80℃

Carrier gas

37 mL/min N2 (Adjust so that the retention time of isoflurane is about 7 minutes.)

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

2.0 μL

View detail

GC

Samples

Pyridine , 2-ethyl-2-phenylmalonediamide , Stearylalcohol ,

Applications

Analysis of primidone using Shinwasorb ～Purity test (3) 2-ethyl-2-phenylmalonediamide～

Column

Silicone OV-17 1.5% Shinwasorb-S 100/120

Column Size

1.6 m x 3.2 mm I.D. Glass

Column temp.

195℃

Carrier gas

31 mL/min N2 (Adjust so that the retention time of stearylalcohol is about 10 minutes.)

Injection port temp.

250°C

Detector temp.

250°C

Detector

FID

Injection volume

2.0 μL

View detail

GC

Samples

Deet, diethyl phthalate in ethanol

Applications

Analysis of deet (Pesticide guidelines) ~Purity test (4) Related substances~

Column

ULBON HR-20M

Column Size

0.2 mm I.D. x 25 m df = 0.1 µmm

Column temp.

170℃

Carrier gas

21 cm/sec He (Adjust so that the retention time of deet is about 10 minutes.)

Injection port temp.

230°C

Detector temp.

230°C

Detector

FID

Injection volume

2.0 μL (Split rate: 1:70)

View detail

GC

Samples

Methanol in ethanol

Applications

Analysis of etidronate disodium using Sunpak-A ~Purity test (4) Methanol~

Column

Sunpak-A 50/80

Column Size

2.1m x3.2 mm I.D. Glass

Column temp.

130℃

Carrier gas

30 mL/min N2 (Adjust so that the retention time of methanol is about 2 minutes.)

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

2-propanol, ethanol in water

Applications

Analysis of sodium aurothiomalate using Sunpak-H ~Purity test (4) Ethanol~

Column

Sunpak-H 80/100

Column Size

3.1m x 3.2 mm I.D. Glass

Column temp.

145℃

Carrier gas

28 mL/min N2 (Adjust so that the retention time of 2-propanol is about 7 minutes.)

Injection port temp.

230°C

Detector temp.

230°C

Detector

FID

Injection volume

2.0 μL

View detail

GC

Samples

water, acetonitrile in methanol

Applications

Analysis of panipenem using Sunpak-A ~Water~

Column

Sunpak-A 80/100

Column Size

2.1m x 3.2 mm I.D. Glass

Column temp.

125℃

Carrier gas

29 mL/min He (Adjust so that the retention time of acetonitrile is about 8 minutes.)

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

Acetone , Ethyl acetate

Applications

Analysis of piperacillin hydrate using Sunpak-H ~(4) Residual solvents~

Column

Sunpak-H 80/100

Column Size

1.1m x 3.2 mm I.D. Glass

Column temp.

145℃

Carrier gas

33 mL/min N2 (Adjust so that the retention time of ethyl acetate is about 4 minutes.)

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

2.0 μL

View detail

GC

Samples

Cyclohexane , Dicyclohexyl phthalate , Etofenprox

Applications

Analysis of etofenprox using Shinwasorb

Column

Silicone OV-225 2.5% Shinwasorb-U 60/80

Column Size

1.1m x 3.2 mm I.D. Glass

Column temp.

240℃

Carrier gas

37 mL/min N₂ (Adjust so that the retention time of dicyclohexyl phthalate is about 8 minutes.)

Injection port temp.

250°C

Detector temp.

250°C

Detector

FID

Injection volume

3.0 μL

View detail

GC

Samples

Etofenprox in Cyclohexane

Applications

Analysis of etofenprox using Shinwasorb -2- ～Purity (3) Related substances～

Column

Silicone OV-225 2.5% Shinwasorb-U 60/80

Column Size

1.1m x 3.2 mm I.D. Glass

Column temp.

240℃

Carrier gas

37 mL/min N₂

Injection port temp.

250°C

Detector temp.

250°C

Detector

FID

Injection volume

3.0 μL

View detail

GC

Samples

o-Dichlorobenzene, m-Bromochlorobenzene in acetone

Applications

Analysis of o-dichlorobenzene using Shinwasorb

Column

PEG20M-TPA 2.5% Shinwasorb-U 60/80

Column Size

3.1 m x 3.2 mm I.D. Glass

Column temp.

115℃

Carrier gas

39 mL/min N₂ (Adjust so that the retention time of o-dichlorobenzene is about 11 minutes.)

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

2.0 μL

View detail