GC

Samples

Mixture of 13 organic solvents

Applications

Measurement of organic solvents using Shinwasorb -1-

Column

PEG1500 12.5% Shinwasorb-U 40/60

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

70℃

Carrier gas

40 mL/min N₂

Injection port temp.

200℃

Detector temp.

200℃

Detector

FID

Injection volume

1.0 μL

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GC

Samples

Mixture of 22 organic solvents

Applications

Measurement of organic solvents using Shinwasorb -2-

Column

PEG1500 12.5% Shinwasorb-U 40/60

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

60～120℃ (4℃/min)

Carrier gas

40 mL/min N₂

Injection port temp.

200℃

Detector temp.

200℃

Detector

FID

Injection volume

1.0 μL

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GC

Samples

Isopropyl iodide , Methylcyclohexane , o-xylene

Applications

Analysis of hydroxypropylcellulose (JP)

Column

ULBON HR-1

Column Size

0.53 mm I.D. x 30 m df = 3.0 µm

Column temp.

40℃ (3 min)～10℃/min～100℃～50℃/min～250℃ (3 min)

Carrier gas

52 cm/sec He

Injection port temp.

180°C

Detector temp.

280°C

Detector

FID

Injection volume

2.0 μL Split rate: 1:50

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GC

Samples

Cyclohexane , N,N-dimethylaniline , Naphthalene ,

Applications

Analysis of ampicillin hydrate using Shinwasorb

Column

Silicone OV-17 1.5% Shinwasorb-S 60/80

Column Size

2.1 m x 2.6 mm I.D. Glass

Column temp.

105℃

Carrier gas

20 mL/min He（adjust so that the retention time of N,N-dimethylaniline is about 5 minutes.)

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

1.0 μL

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GC

Samples

Cyclohexane , Ethyl acetate , 2-propanol ,

Applications

Analysis of lenampicillin hydrochloride using Shinwasorb

Column

Quadrol 5% Shinwasorb-S 60/80

Column Size

3.1 m x 3.2 mm I.D. Glass

Column temp.

100℃

Carrier gas

70 mL/min N₂ (Adjust so that the retention time of cyclohexane is about 1 minute.)

Injection port temp.

160°C

Detector temp.

160°C

Detector

FID

Injection volume

4.0 μL

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GC

Samples

Cyclohexane , Dicyclohexyl phthalate , Etofenprox

Applications

Analysis of etofenprox using Shinwasorb

Column

Silicone OV-225 2.5% Shinwasorb-U 60/80

Column Size

1.1m x 3.2 mm I.D. Glass

Column temp.

240℃

Carrier gas

37 mL/min N₂ (Adjust so that the retention time of dicyclohexyl phthalate is about 8 minutes.)

Injection port temp.

250°C

Detector temp.

250°C

Detector

FID

Injection volume

3.0 μL

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GC

Samples

Etofenprox in Cyclohexane

Applications

Analysis of etofenprox using Shinwasorb -2- ～Purity (3) Related substances～

Column

Silicone OV-225 2.5% Shinwasorb-U 60/80

Column Size

1.1m x 3.2 mm I.D. Glass

Column temp.

240℃

Carrier gas

37 mL/min N₂

Injection port temp.

250°C

Detector temp.

250°C

Detector

FID

Injection volume

3.0 μL

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LC

Samples

Sucrose , Lactose , Glucose , Xylose , Galactose , Fructose , Inositol

Applications

Sugar and alditol

Column

ULTRON PS-80P

Column Size

300 mm L × 8.0 mm I.D.

Mobile phase

H2O

Frow rate

1.0 mL/min

Column temp.

80°C

Pressure

2.0 MPa

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LC

Samples

Erythritol , Xylitol , Fructose , Glucose , Sorbitol , Sucrose , Inositol , Maltose , Maltitol , Lactose , Lactitol

Applications

Analysis of saccharides and sweeteners

Column

ULTRON AF-HILIC-CD

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

A: 100mM CH3CO2NH4 (pH6.8) /CH3CN = 10/90, B: 100mM CH3CO2NH4 (pH6.8) /CH3CN = 70/30

Frow rate

0.32 mL/min

Column temp.

40°C

Injection volume

1.0 µL

Diluent

H2O /CH3CN = 50/50

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