GC

Samples

dl-Camphor , l-Menthol , Methyl Salicylate , Thymol

Applications

The component of the liniment

Column

Thermon-3000 10% Chromosorb W 80-100 (AW-DMCS)

Column Size

3.1m×3.2mm

Column temp.

175°C

Carrier gas

N2,60ml/min

Injection port temp.

250°C

Detector temp.

250°C(FID)

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GC

Samples

α-Pinene , β-Pinene , Limonene , Octyl Aldehyde , Nonyl Aldehyde , Citronellal , Decyl Aldehyde , Linalool , Linalyl Acetate , Isobornyl Acetate(Citronellol) , Menthol , Benzyl Acetate , Perillaldehyde , Geraniol , α-Ionone , Rose-P , C12-Alcohol , Anisaldehyde , Methyl Cinnamate , Ethyl Cinnamate , Eugenol , Heliotropin , DEP , Vanillin , Benzyl Benzoate , Benzyl Salicylate

Applications

The mixed sample of perfume component

Column

Thermon-3000 5% Chromosorb W 80-100 (AW-DMCS)

Column Size

3.1m×3.2mm

Column temp.

80°C→250°C(6°C/min)

Carrier gas

N2,60ml/min

Injection port temp.

290°C

Detector temp.

280°C(FID)

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GC

Samples

β-Pinene , Limonene , Linalool , Linalyl Acetate , Benzyl Acetate , α-Ionene , Phenethyl Alcohol , Lauryl Alcohol , Eugenol , Diethyl Phthalate , Vanillin , Benzyl Salicylate

Applications

perfume (2)

Column

ULBON HR-Thermon-600T

Column Size

50m×0.25mm

Column temp.

70°C→230°C(4°C/min)

Carrier gas

He,1.1ml/min

Detector temp.

250°C(FID)

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GC

Samples

Fragrance

Applications

Measurements of fragrance using Shinwasorb

Column

Thermon-3000 5% Shinwasorb-S 80/100

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

80～260℃（6℃/min)

Carrier gas

50 mL/min N₂

Injection port temp.

280℃

Detector temp.

280℃

Detector

FID

Injection volume

1.0 μL

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GC

Samples

Ethanol , Dl-camphor , Methyl salicylate ,

Applications

Analysis of dl-camphor using Shinwasorb

Column

PEG 20M 5% Shinwasorb-S 60/80

Column Size

3.1m×3.2mm glass

Column temp.

160°C

Carrier gas

45 mL/min N2

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

2.0 μL

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LC

Samples

Methyl salicylate , Ethyl salicylate , Propyl salicylate , Butyl salicylate

Applications

The elution behavior of the acid sample

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

CH3CN/H2O = 70/30

Frow rate

1.0 mL/min

Column temp.

30°C

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LC

Samples

Salicylic acid , Diphenhydramine , Methyl salicylate , α-Camphor , Thymol

Applications

The component of the anti-inflammatory agent

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

10 mM Phosphoric acid buffer(pH 2.6) + 20 mM Heptane sodium sulphonate/CH3OH/CH3CN = 3/2/2

Frow rate

1.0 mL/min

Column temp.

45°C

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