GC

Samples

Acetic Acid , Propionic Acid , Isobutyric Acid , Butyric Acid . Isovaleric Acid , Isocaproic Acid , Caproic Acid , Enanthic Acid

Applications

[ DEGS + H3PO4 ] Apprication of Lower free fatty acid

Column

DEGS+H3PO4(10%+1%) Chromosorb W 80-100 (AW-DMCS)

Column Size

2.1m×3.2mm

Column temp.

160°C

Carrier gas

N2,50ml/min

Injection port temp.

250°C

Detector temp.

250°C(FID)

View detail

GC

Samples

Sorbic Acid , Dehydroacetic Acid , Benzoic Acid , trans-Stilbene

Applications

Antiseptics (2)

Column

DEGS+H3PO4(2%+0.5%) Chromosorb W 60-80 (AW-DMCS)

Column Size

2.1m×3.2mm

Column temp.

200°C

Carrier gas

N2,40ml/min

Injection port temp.

260°C

Detector temp.

260°C(FID)

View detail

GC

Samples

Sorbic Acid , Dehydroacetic Acid , Benzoic Acid , trans-Stilbene(I.S.)

Applications

Antiseptics (1)

Column

DEGS+H3PO4(5%+1%) Chromosorb W 60-80 (AW-DMCS)

Column Size

2.1m×3.2mm

Column temp.

185°C

Carrier gas

N2,60ml/min

Injection port temp.

260°C

Detector temp.

260°C(FID)

View detail

GC

Samples

Acetic Acid , Propionic Acid , Isobutyric Acid , Butyric Acid , Isovaleric Acid , Valeric Acid , Isocaproic Acid , Caproic Acid

Applications

Free lower fatty acids (4) (each 100ppm)

Column

FFAP+H3PO4(0.3%+0.3%) Graphitecarbon 60〜80

Column Size

1.6m×3.2mm

Column temp.

80°C→220°C(16°C/min)

Carrier gas

N2,60ml/min

Injection port temp.

260°C

Detector temp.

260°C(FID)

View detail

GC

Samples

Acetic Acid , Propionic Acid , Isobutyric Acid , Butyric Acid , Isovaleric Acid , Isocaproic Acid , Caproic Acid , Enanthic Acid

Applications

[ Thermon-1000+H3PO4 ] Apprication of Lower free fatty acid

Column

Thermon-1000+H3PO4(10%+1%) Chromosorb W 80-100 (AW-DMCS)

Column Size

2.1m×3.2mm

Column temp.

160°C

Carrier gas

N2,50ml/min

Injection port temp.

250°C

Detector temp.

250°C(FID)

View detail

GC

Samples

Acetic acid , Propionic acid , Isobutyric acid , Butyric acid , Isovaleric acid , Valeric acid , Isocaproic acid , Capric acid , Enanthic acid

Applications

Measurement of short-chain free fatty acids using Shinwasorb -1-

Column

Thermon-1000+H3PO4 2.5+0.25% Shinwasorb-U 60/80

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

150℃

Carrier gas

50 mL/min N₂

Injection port temp.

250℃

Detector temp.

240℃

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

Sorbic acid , Dehydroacetic acid , Benzoic acid , trans-Stilbene

Applications

Analysis of preservatives using Shinwasorb -1-

Column

DEGS+H3PO4 5.0+0.5% Shinwasorb-S 40/60

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

185℃

Carrier gas

50 mL/min N₂

Injection port temp.

260℃

Detector temp.

260℃

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

preservatives

Applications

Analysis of preservatives using Shinwasorb -2-

Column

Advance-DS+H3PO4 2+0.25% Shinwasorb-S 60/80

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

200℃

Carrier gas

50 mL/min N₂

Injection port temp.

260℃

Detector temp.

260℃

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

n-valeric acid , valproic acid

Applications

Analysis of valproate sodium using Shinwasorb

Column

DEGA+H3PO4 2.5+0.5% Shinwasorb-S 80/100

Column Size

2.1m×3.2mm glass

Column temp.

145°C

Carrier gas

35 mL/min N2

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

2.0 μL

View detail

LC

Samples

Atenolol

Applications

Atenolol

Column

ULTRON ES-PhCD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 90/10

Frow rate

0.3 mL/min

Column temp.

25°C

View detail

LC

Samples

Methylephedrine hydrochloride , Noscapine , Thiamine , Dextromethorphan , Carbinoxamine maleate

Applications

The component of the cold remedy (1)

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

CH3CN/H2O/H3PO4 = 510/490/1 + 0.5% Sodium dodecyl sulfate

Frow rate

1.0 mL/min

Column temp.

50°C

View detail

LC

Samples

Nicotinic acid , Nicotinic acid amide , Calcium pantothenate , Pyridoxine hydrochloride , Riboflavin phosphate , Thiamine , Folic acid , Biotin , Riboflavin

Applications

The water-soluble vitamin

Column

ULTRON VX-ODS

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM H3PO4/5 mM Sodium 1-hexanesulfonate = 91/9

Frow rate

1.0 mL/min

Column temp.

45°C

View detail

LC

Samples

2-(4-Hydroxyphenoxy)propionic acid

Applications

2-(4-Hydroxyphenoxy)propionic acid

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4(pH 3.0)/CH3CN = 90/10

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Bepridil hydrochloride

Applications

Bepridil hydrochloride

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4(pH 3.0)/CH3CN = 95/5

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Bicalutamide

Applications

Bicalutamide

Column

ULTRON ES-CD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4(pH 3.0)/C2H5OH = 95/5

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Bicalutamide

Applications

Bicalutamide

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4(pH 3.0)/CH3CN = 87/13

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Duloxetine hydrochloride

Applications

Duloxetine hydrochloride

Column

ULTRON ES-PhCD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4(pH 3.0)/CH3CN = 65/35

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Tadalafil

Applications

Analyses of Tadalafil in ULTRON ES-OVM series.(Faster analyses with 3µm particles)

Column

ULTRON ES-OVM

Column Size

(1)150 mm L × 4.6 mm I.D.　(2)100 mm L × 3.0 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

(1)2.0 µL　(2)0.5 µL

Diluent

methanol

View detail

LC

Samples

Tadalafil

Applications

Analyses of Tadalafil in ULTRON ES-OVM series.(Greater analytical performance with 3µm particles)

Column

ULTRON ES-OVM

Column Size

(1)150 mm L × 4.6 mm I.D.　(2)100 mm L × 3.0 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15

Frow rate

(1)1.0 mL/min　(2)0.28 mL/min

Column temp.

25°C

Injection volume

(1)2.0 µL　(2)0.5 µL

Diluent

methanol

View detail

LC

Samples

Sertraline hydrochloride

Applications

Analysis of Sertraline hydrochloride

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

Diluent

methanol

View detail

LC

Samples

Nisoldipine

Applications

Analysis of Nisoldipine

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 88/12

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

Diluent

ethanol

View detail

LC

Samples

Cinacalcet hydrochloride

Applications

Analysis of Cinacalcet hydrochloride

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 93/7

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

Diluent

ethanol

View detail

LC

Samples

Atorvastatin calcium

Applications

Analysis of Atorvastatine calcium

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM K2HPO4 + H3PO4 (pH 7.5)/CH3OH = 85/15

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

Diluent

ethanol

View detail

LC

Samples

Montelukast sodium

Applications

Analysis of Montelukast sodium

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3OH = 60/40

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

Diluent

methanol

View detail

LC

Samples

Rebamipide

Applications

Analysis of Rebamipide

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 87/13

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

1.0 µL

Diluent

methanol

View detail

LC

Samples

Sulconazole nitrate

Applications

Analysis of Sulconazole nitrate

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3OH = 86/14

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

Diluent

methanol

View detail

LC

Samples

2-(4-Hydroxyphenoxy)propionic acid

Applications

Analysis of 2-(4-Hydroxyphenoxy)propionic acid

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 90/10

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

Diluent

water

View detail

LC

Samples

3,3-Dimethyl-4-phenyl-2-azetidinone

Applications

Analysis of 3,3-Dimethyl-4-phenyl-2-azetidinone

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/C2H5OH = 95/5

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

Diluent

methanol

View detail

LC

Samples

2-Phenoxypropionic acid

Applications

Analysis of 2-Phenoxypropionic acid

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/C2H5OH = 90/10

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

Diluent

water

View detail

LC

Samples

Tadalafil

Applications

Analysis of tadalafil

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

Diluent

methanol

View detail

LC

Samples

Tadalafil

Applications

Analysis of Tadalafil

Column

ULTRON ES-OVM

Column Size

100 mm L × 3.0 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

0.5 µL

Diluent

methanol

View detail

LC

Samples

Tadalafil

Applications

Analysis of Tadalafil

Column

ULTRON ES-OVM

Column Size

100 mm L × 3.0 mm I.D.

Mobile phase

20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15

Frow rate

0.28 mL/min

Column temp.

25°C

Injection volume

0.5 µL

Diluent

methanol

View detail

LC

Samples

Linolenic acid , Myristic acid , Palmitoleic acid , Arachidonic acid , Linoleic acid , Palmitic acid , Oleic acid

Applications

Analysis of Long-chain fatty acid

Column

STR ODS-Ⅱ

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

CH3CN/0.1% H3PO4 aq = 80/20

Frow rate

1.0 mL/min

Column temp.

40°C

Injection volume

5 µL

Diluent

ethyl acetate

View detail