GC

Samples

n-Nonane , n-Hedecane , n-Tridecane , n-Pentadecane , n-Heptadecane , n-Nonadecane , n-Heneicosane , Pyrene(I.S.)

Applications

The mixed sample of kerosene and light oil

Column

Silicone SE-52 5% Shimalite W 60-80 (AW)

Column Size

2.5m×3mm(SUS)

Column temp.

80°C→250°C(6°C/min)

Carrier gas

N2,50ml/min

Injection port temp.

270°C

Detector temp.

270°C(FID)

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GC

Samples

decane , undecane , dodecane , tridecane , tetradecane , pentadecane , hexadecane , heptadecane , octadecane , nonadecane , eicosane , heneicosane , docosane

Applications

Analysis of mixture of kerosene and gas oil using Shinwasorb

Column

Silicone SE-52 5% Shinwasorb-U 40/60

Column Size

2.5 m x 3.0 mm I.D. Stainless steel

Column temp.

80～250℃ (6℃/min), 250℃ (12 min hold)

Carrier gas

50 mL/min N2

Injection port temp.

270°C

Detector temp.

270°C

Detector

FID

Injection volume

1.0 μL

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GC

Samples

N,N-dimethylformamide , Triphenylantimony , Spectinomycin ,

Applications

Analysis of spectinomycin hydrochloride hydrate using Shinwasorb

Column

Silicone SE-52 2.5% Shinwasorb-S 80/100

Column Size

0.6 m x 3.2 mm I.D. Glass

Column temp.

180℃

Carrier gas

37 mL/min N2

Injection port temp.

215℃

Detector temp.

220℃ 　

Detector

FID

Injection volume

1.0 μL

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