GC

Samples

Ethyl Acetate , Acetaldehyde-2,4-Dinitrophenylhydrazone

Applications

Acetaldehyde -2,4- dinitrophenylhydrazone

Column

Silicone OV-17 1% Chromosorb W 80-100 (AW-DMCS)

Column Size

2.1m×3.2mm

Column temp.

220°C

Carrier gas

N2,60ml/min

Injection port temp.

270°C

Detector temp.

270°C(FID)

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GC

Samples

Estrone , Estriol

Applications

Estrone and Estriol

Column

Silicone OV-17 1.5% Shimalite W 80-100 (AW-DMCS)

Column Size

1.6m×3.2mm

Column temp.

260°C

Carrier gas

N2,50ml/min

Injection port temp.

290°C

Detector temp.

290°C(FID)

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GC

Samples

α-BHC , γ-BHC , β-BHC , δ-BHC , Parathion , PP´-DDE , Endrin , PP´-DDD , PP´-DDT , EPN

Applications

Chlorinated pesticide in green tea

Column

Silicone OV-17 2% Chromosorb W 80-100 (AW-DMCS)

Column Size

2.1m×3.2mm

Column temp.

200°C

Carrier gas

N2,60ml/min

Injection port temp.

270°C

Detector temp.

270°C(ECD)

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GC

Samples

PCBs

Applications

Analysis of PCBs using Shinwasorb

Column

Silicone OV-17 2％ Shinwasorb-U 60/80　　

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

210℃

Carrier gas

50 mL/min N₂

Injection port temp.

260℃

Detector temp.

260℃

Detector

ECD

Injection volume

4.0 μL

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GC

Samples

Dichlorvos (DDVP) , Methyldemeton , Methyl parathion , Parathion , EPN

Applications

Measurement of organophosphorus compounds using Shinwasorb

Column

Silicone OV-17 1% Shinwasorb-S 60/80

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

180-250℃ (8℃/min)

Carrier gas

50 mL/min N₂

Injection port temp.

260℃

Detector temp.

260℃

Detector

FPD

Injection volume

1.0 μL

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GC

Samples

homatropine hydrobromide , atropine

Applications

Analysis of opium alkaloid atropine using Shinwasorb

Column

Silicone OV-17 1% Shinwasorb-S 60/80

Column Size

1.6m×3.2mm glass

Column temp.

210°C

Carrier gas

40 mL/min N2

Injection port temp.

270°C

Detector temp.

270°C

Detector

FID

Injection volume

2.0 μL

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GC

Samples

homatropine hydrobromide , scopolamine

Applications

Analysis of opium alkaloid scopolamine using Shinwasorb

Column

Silicone OV-17 1% Shinwasorb-S 60/80

Column Size

1.6m×3.2mm glass

Column temp.

210°C

Carrier gas

45 mL/min N2

Injection port temp.

250°C

Detector temp.

250°C

Detector

FID

Injection volume

2.0 μL

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GC

Samples

Cyclohexane , N,N-dimethylaniline , Naphthalene ,

Applications

Analysis of ampicillin hydrate using Shinwasorb

Column

Silicone OV-17 1.5% Shinwasorb-S 60/80

Column Size

2.1 m x 2.6 mm I.D. Glass

Column temp.

105℃

Carrier gas

20 mL/min He（adjust so that the retention time of N,N-dimethylaniline is about 5 minutes.)

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

1.0 μL

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GC

Samples

Pyridine , 2-ethyl-2-phenylmalonediamide , Stearylalcohol ,

Applications

Analysis of primidone using Shinwasorb ～Purity test (3) 2-ethyl-2-phenylmalonediamide～

Column

Silicone OV-17 1.5% Shinwasorb-S 100/120

Column Size

1.6 m x 3.2 mm I.D. Glass

Column temp.

195℃

Carrier gas

31 mL/min N2 (Adjust so that the retention time of stearylalcohol is about 10 minutes.)

Injection port temp.

250°C

Detector temp.

250°C

Detector

FID

Injection volume

2.0 μL

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GC

Samples

Acetone , Allethrin , Cinerin I , Jasmolin I , Pyrethrin I , Cinerin II , Jasmolin II , Pyrethrin II

Applications

Analysis of pyrethrum extract using Shinwasorb

Column

Silicone OV-17 1% Shinwasorb-S 80/100

Column Size

1.1 m x 3.2 mm I.D. Glass

Column temp.

205℃

Carrier gas

35 mL/min N₂（Adjust so that the retention time of Allethrin is about 3 minutes.)

Injection port temp.

230°C

Detector temp.

230°C

Detector

FPD

Injection volume

1.0 μL

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