GC

Samples

IPA , Methyl Cellosolve , n-Butanol , 1-Methoxy-2-Propanol , Ethyl Cellosolve , Butyl Cellosolve

Applications

Lower alcohol and Cellosolves

Column

Thermon-1000 5% Sunpak-A

Column Size

2.1m×3.2mm

Column temp.

170°C→220°C(6°C/min)

Carrier gas

N2,50ml/min

Injection port temp.

260°C

Detector temp.

260°C(FID)

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GC

Samples

Cyclohexane , Ethyl acetate , 2-propanol ,

Applications

Analysis of lenampicillin hydrochloride using Shinwasorb

Column

Quadrol 5% Shinwasorb-S 60/80

Column Size

3.1 m x 3.2 mm I.D. Glass

Column temp.

100℃

Carrier gas

70 mL/min N₂ (Adjust so that the retention time of cyclohexane is about 1 minute.)

Injection port temp.

160°C

Detector temp.

160°C

Detector

FID

Injection volume

4.0 μL

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GC

Samples

Enflurane , 2-propanol ,

Applications

Analysis of enflurane using Shinwasorb

Column

DEGS 10% Shinwasorb-S 60/80

Column Size

3.1 m x 3.2 mm I.D. Glass

Column temp.

80℃

Carrier gas

32 mL/min He (Adjust so that the retention time of enflurane is about 3 minutes.)

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

5.0 μL

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GC

Samples

2-propanol, ethanol in water

Applications

Analysis of sodium aurothiomalate using Sunpak-H ~Purity test (4) Ethanol~

Column

Sunpak-H 80/100

Column Size

3.1m x 3.2 mm I.D. Glass

Column temp.

145℃

Carrier gas

28 mL/min N2 (Adjust so that the retention time of 2-propanol is about 7 minutes.)

Injection port temp.

230°C

Detector temp.

230°C

Detector

FID

Injection volume

2.0 μL

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GC

Samples

Diethyl ether , n-Hexane , Methanol , Methyl acetate , 2-Propanol , Ethyl acetate , Tetrahydrofuran , 2-Butanol , iso-Butanol , Toluene , n-Butyl acetate , Methyl n-butyl ketone , iso-Amyl alcohol , Ethylbenzene , m-Xylene , p-Xylene , o-Xylene , Styrene monomer ,

Applications

Measurement of organic solvents using SBS-120

Column

SBS-120 12% Shincarbon-A2 80/100

Column Size

3.1 m x 3.2 mm I.D. Glass

Column temp.

90℃

Carrier gas

40 mL/min N₂

Injection port temp.

230℃

Detector temp.

230℃

Detector

FID

Injection volume

1.0 μL

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LC

Samples

Alprenolol

Applications

β-Blocking agent

Column

ULTRON ES-PEPSIN

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 5.0)/C2H5OH = 95/5

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

0.9 µL (0.6 mg/mL)

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LC

Samples

Bufetolol

Applications

β-Blocking agent

Column

ULTRON ES-PEPSIN

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 5.0)/C2H5OH = 95/5

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

1.0 µL (ca. 1 mg/mL)

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LC

Samples

Alprenolol

Applications

Alprenolol

Column

ULTRON ES-PhCD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 4.6)/CH3CN = 80/20

Frow rate

1.2 mL/min

Column temp.

25°C

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LC

Samples

Chlorphenamine maleate

Applications

Analysis of Chlorphenamine maleate using the ULTRON ES-Amy-DM

Column

ULTRON ES-Amy-DM

Column Size

250 mm L × 4.6 mm I.D.

Mobile phase

n-Hexane/IPA/TFA = 95/5/0.1

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

10 µL

Diluent

2-propanol + 0.2% diethanolamine

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LC

Samples

Chlorphenamine maleate

Applications

Analysis of Chlorphenamine maleate using the ULTRON ES-AmyCL-DM

Column

ULTRON ES-AmyCL-DM

Column Size

250 mm L × 4.6 mm I.D.

Mobile phase

n-Hexane/IPA/DEA = 95/5/0.1

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

10 µL

Diluent

2-propanol + 0.2% diethanolamine

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LC

Samples

Universal primer T7

Applications

Analysis of Universal primer T7 using the ULTRON AF-HILIC-CD “Difference in retention time by addition of different alcohols to mobile phase”

Column

ULTRON AF-HILIC-CD

Column Size

150 mm L × 2.0 mm I.D.

Frow rate

0.15 mL/min

Column temp.

30°C

Injection volume

0.5 µL

Diluent

CH3CN/TE buffer※ = 70/30

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