GC

Samples

Diethyl Phthalate , Di-iso-Butyl Phthalate , Di-n-Butyl Phthalate , Di-n-Amyl Phthalate , Diheptyl Phthalate , Dioctyl Phthalate

Applications

Phthalic acid ester (2) (200ppm)

Column

Thermon-3000 2% Chromosorb W 80-100 (AW-DMCS)

Column Size

2.1m×3.2mm

Column temp.

215°C

Carrier gas

N2,65ml/min

Injection port temp.

260°C

Detector temp.

260°C(FID)

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GC

Samples

Dimethyl Phthalate , Diethyl Phthalate , Diallyl Phthalate , Di-iso-Butyl Phthalate , Di-n-Butyl Phthalate , Di-n-Amyl Phthalate , Di-2-Ethylhexyl Phthalate , Di-n-Octyl Phthalate

Applications

Phthalic acid ester (1)

Column

ULBON HR-1

Column Size

25m×0.25mm(0.25μm)

Column temp.

180°C→300°C(6°C/min)

Carrier gas

He,0.98ml/min

Detector temp.

320°C(FID)

Injection volume

0.5μl

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GC

Samples

n-Butyl Formate , n-Butyl Acetate , n-Butyl Propionate , n-Butyl iso-Butyrate , n-Butyl n-Butyrate , n-Butyl Crotonate , n-Butyl n-Caproate , n-Butyl Lactate , n-Butyl n-Caprate , Di-n-Butyl Oxalate , n-Butyl Benzoate , Di-n-Butyl Malonate , Di-n-Butyl Fumarate , Di-n-Butyl Succinate , Di-n-Butyl Maleate , Di-n-Butyl Adipate , Di-n-Butyl Maleate , Di-n-Butyl Phthalate , Di-n-Butyl Sebacate , Di-n-Butyl Isophthalate , Di-n-Butyl Terephthalate , Tri-n-Butyl Citrate

Applications

Organic acid butyl ester

Column

ULBON HR-20M

Column Size

25m×0.25mm(0.25μm)

Column temp.

80°C→240°C(4°C/min)

Carrier gas

He,1.1ml/min

Detector temp.

250°C(FID)

Injection volume

1.0μm

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GC

Samples

Ethyl acetate , di-n-butyl phthalate , Teprenone (mono-cis isomer) , Teprenone (all-trans isomer) , ,

Applications

Analysis of teprenone using Shinwasorb -1-

Column

FFAP 5% Shinwasorb-U 80/100

Column Size

2.1m×3.2mm glass

Column temp.

235°C

Carrier gas

47 mL/min N2

Injection port temp.

270°C

Detector temp.

270°C

Detector

FID

Injection volume

2.0 μL

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GC

Samples

Ethyl acetate , di-n-butyl phthalate , Teprenone (mono-cis isomer) , Teprenone (all-trans isomer) , ,

Applications

Analysis of teprenone using Shinwasorb -2-

Column

FFAP 5% Shinwasorb-U 80/100

Column Size

2.1m×3.2mm glass

Column temp.

235°C

Carrier gas

47 mL/min N2

Injection port temp.

270°C

Detector temp.

270°C

Detector

FID

Injection volume

2.0 µL

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GC

Samples

Diazinon, Di-n-butyl phthalate in Acetone

Applications

Analysis of diazinon using Shinwasorb

Column

Silicone OV-11 10% Shinwasorb-U 60/80

Column Size

1.6 m x 3.2 mm I.D. Glass

Column temp.

200℃

Carrier gas

25 mL/min N₂（Adjust so that the retention time of diazinon is about 7 minutes.)

Injection port temp.

230°C

Detector temp.

230°C

Detector

FID

Injection volume

3.0 μL

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GC

Samples

Anhydrous caffeine, Fenitrothion in Acetone

Applications

Analysis of Fenitrothion Emulsifiable Concentrate using Shinwasorb

Column

Silicone OV-210 3% Shinwasorb-S 80/100

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

175℃

Carrier gas

51 mL/min N₂（Adjust so that the retention time of Anhydrous caffeine is about 10 minutes.)

Injection port temp.

230°C

Detector temp.

230°C

Detector

FID

Injection volume

2.0 μL

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