GC

Samples

Trimethylamine , Dimethylamine , Monomethylamine

Applications

Mono-, di-, trimethylamine

Column

Diglycerol+TEP+KOH(15%+15%+2%) Chromosorb W 80-100 (AW-DMIS)

Column Size

3.1m×3.2mm

Column temp.

70°C

Carrier gas

N2,60ml/min

Injection port temp.

230°C

Detector temp.

230°C(FID)

View detail

GC

Samples

Ethyleneglycol , Diethyleneglycol , Triethyleneglycol

Applications

Glycols (1)

Column

TENAX TA 60-80

Column Size

1.1m×3.2mm

Column temp.

180°C→210°C(3°C/min)

Carrier gas

N2,50ml/min

Injection port temp.

260°C

Detector temp.

260°C(FID)

View detail

GC

Samples

Propyleneglycol , Ethyleneglycol , Decyl Alcohol , 1,4-Butanediol , Diethyleneglycol , Lauryl Alcohol , Myristyl Alcohol , Triethyleneglycol , Cetyl Alcohol , Stearyl Alcohol

Applications

Glycol and higher alcohol

Column

Thermon-3000 1% Shimalite TPA 60-80

Column Size

1.1m×3.2mm

Column temp.

90°C→180°C(5°C/min)

Carrier gas

N2,60ml/min

Injection port temp.

260°C

Detector temp.

260°C(FID)

View detail

GC

Samples

Triglyceride

Applications

The oil ball

Column

ULBON HR-TGC1

Column Size

25m×0.25mm(0.1μm)

Column temp.

100°C→390°C(8°C/min)

Carrier gas

He,1.5kg/cm2

Detector temp.

390°C(FID)

Injection volume

1μl

View detail

GC

Samples

Triglyceride

Applications

Calnaubawax

Column

ULBON HR-TGC1

Column Size

25m×0.25mm(0.1μm)

Column temp.

250°C→380°C(5°C/min)

Carrier gas

He,1.3kg/cm2

Detector temp.

390°C(FID)

Injection volume

0.2μl

View detail

GC

Samples

Triglyceride

Applications

Triglyceride

Column

ULBON HR-TGC1

Column Size

25m×0.25mm(0.1μm)

Column temp.

250°C→380°C(5°C/min)

Carrier gas

He,1.3kg/cm2

Detector temp.

390°C(FID)

Injection volume

0.2μl

View detail

GC

Samples

Trimethylamine , Dimethylamine , Methylamine

Applications

Analysis of methylamines using Shinwasorb

Column

Diglycerol+TEP+KOH 7.5+7.5+1% Shinwasorb-S 60/80

Column Size

3.1 m x 3.2 mm I.D. Glass

Column temp.

70℃

Carrier gas

50 mL/min N₂

Injection port temp.

220℃

Detector temp.

220℃

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

Mixture of 22 organic solvents

Applications

Measurement of organic solvents using Shinwasorb -2-

Column

PEG1500 12.5% Shinwasorb-U 40/60

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

60～120℃ (4℃/min)

Carrier gas

40 mL/min N₂

Injection port temp.

200℃

Detector temp.

200℃

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

Propyleneglycol , 1,3-propanediol

Applications

Measurement of food additives using Sunpak-A

Column

Sunpak-A 50/80

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

180℃

Carrier gas

50 mL/min N₂

Injection port temp.

200℃

Detector temp.

230℃

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

Propyleneglycol , 1,3-propanediol

Applications

Measurement of food additives using Sunpak-A

Column

Sunpak-A 50/80

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

180℃

Carrier gas

50 mL/min N₂

Injection port temp.

200℃

Detector temp.

230℃

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

Ethylene glycol , Diethylene glycol

Applications

Analysis of macrogol 400 using Shinwasorb

Column

Sorbitol 3% Shinwasorb-S 80/100

Column Size

1.6 m x 3.2 mm I.D. Glass

Column temp.

160℃

Carrier gas

47 mL/min N2

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

2.0 μL

View detail

GC

Samples

Acetone , Allethrin , Di(2-ethylhexyl) phthalate

Applications

Analysis of allethrin using Shinwasorb Part 3

Column

Diethyleneglycol Succinate (DEGS) 2.5% Shinwasorb-U 80/100

Column Size

1.1 m x 3.2 mm I.D. Glass

Column temp.

200℃

Carrier gas

36 mL/min N₂ (Adjust so that the retention time of allethrin is about 8 minutes.)

Injection port temp.

230°C

Detector temp.

230°C

Detector

FID

Injection volume

1.0 μL

View detail

LC

Samples

Chlorphenesin

Applications

Muscle relaxant

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20mM KH2PO4 (pH 5.5)

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Chlorphenesin

Applications

Muscle relaxant

Column

ULTRON ES-PhCD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

20 mM KH2PO4 (pH 4.6)/CH3CN = 70/30

Frow rate

0.6 mL/min

Column temp.

9°C

View detail

LC

Samples

Ethylene glycol , Diethylene glycol , Methanol , Ethanol , Isopropyl alcohol

Applications

Alcohols

Column

ULTRON PS-80H

Column Size

300 mm L × 8.0 mm I.D.

Mobile phase

H2O

Frow rate

1.0 mL/min

Column temp.

60°C

Pressure

2.5 MPa

Injection volume

6.0 µL (10 mg/mL)

View detail

LC

Samples

Citric acid , Tartaric acid , Malic acid , Malonic acid , Succinic acid , Glycolic acid , Formic acid , Lactic acid , Acetic acid , Fumaric acid , Adipic acid , Pyroglutamic acid , Propionic acid , Acrylic acid , Pivalic acid , Methacrylic acid , Crotonic acid

Applications

Elution position of the aliphatic organic acid

Column

ULTRON PS-80H

Column Size

300 mm L × 8.0 mm I.D. + 300 mm L × 8.0 mm I.D.

Mobile phase

HClO4aq. (pH 2.1)

Frow rate

1.0 mL/min

Column temp.

60°C

View detail

LC

Samples

Maltotriose , Maltose , Glucose , Glycerol , Ethanol

Applications

Sake

Column

ULTRON PS-80N

Column Size

300 mm L × 8.0 mm I.D.

Mobile phase

H2O

Frow rate

1.0 mL/min

Column temp.

60°C

Pressure

2.2 MPa

Injection volume

10 µL (undiluted solution)

View detail

LC

Samples

Aspartic acid , Glutamic acid , Serine , Glycine , Histidine , Arginine , Threonine , Alanine , Proline , Tyrosine , Valine , Methionine , Cysteine-cysteine , Isoleucine , Leucine , Phenylalanine , Lysine

Applications

Analysis of the PTC amino acid

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

A: CH3COONa (pH 6.5)/CH3CN = 93/7, B: CH3CN/H2O = 4/1

Frow rate

1.0 mL/min

Column temp.

40°C

View detail

LC

Samples

Iprodione, Bensulide

Applications

Iprodione, Bensulide

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

CH3CN/H2O = 60/40

Frow rate

1.0 mL/min

Column temp.

40°C

View detail

LC

Samples

Hippuric acid , o-Methyl hippuric acid , p-Methyl hippuric acid , m-Methyl hippuric acid

Applications

Hippuric acid

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM Phosphoric acid buffer (pH 2.5) + 10 mM β-Cyclodextrin/CH3CN = 8/1

Frow rate

1.0 mL/min

Column temp.

50°C

View detail

LC

Samples

Glycyrrhetic acid , Propyl paraben

Applications

Glycyrrhizin in the licorice end

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

15 times dilution Acetic acid aqueous solution/CH3CN = 3/2

Frow rate

0.7 mL/min

Column temp.

ambient

View detail

LC

Samples

Cholic acid , Glycocholic acid , Taurocholic acid , Chenodeoxycholic acid , Glycochenodeoxycholic acid , Deoxycholic acid , Taurochenodeoxycholic acid , Taurodeoxycholic acid

Applications

Bile acid

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

CH3CN/30 mM (NH4)2HPO4(Ajusted to pH 7.2 with NH4H2PO4), A: 10/90, B: 50/50

Frow rate

1.0 mL/min

Column temp.

40°C

View detail

LC

Samples

Glycyrrhizin

Applications

Glycyrrhizin

Column

ULTRON VX-ODS

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4(pH 4.6)/CH3CN = 7/3

Frow rate

1.0 mL/min

Column temp.

30°C

View detail

LC

Samples

Glycyrrhetic acid

Applications

Glycyrrhetic acid

Column

ULTRON VX-ODS

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4(pH 4.6)/CH3CN = 1/4

Frow rate

1.0 mL/min

Column temp.

30°C

View detail

LC

Samples

Allantoin , Xanthine , Hypoxanthine , Uric acid

Applications

Uric acid metabolites

Column

ULTRON AF-HILIC-CD

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

10 mM CH3CO2NH4(pH 4.7)/CH3CN = 10/90

Frow rate

0.35 mL/min

Column temp.

30°C

Injection volume

1.0 µL

View detail

LC

Samples

Urea , Xanthine , Lactic acid , Creatinine , Uric acid

Applications

Sweat Composition

Column

ULTRON AF-HILIC-CD (PLSS)

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

10 mM HCO2NH4(pH 3.0)/CH3CN = 10/90

Frow rate

0.30 mL/min

Column temp.

30°C

Injection volume

1.0 µL

View detail

LC

Samples

(CYS)2 , LYS , ARG , HIS , ASP , GLU , GLN , ASN , GLY , SER , ALA , THR , PRO , TYR , VAL , PHE , MET , TRP , LEU+ILE

Applications

Analysis of underivatized amino acids by LC/MS/MS

Column

ULTRON AF-HILIC-CD (PLSS)

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

A: 100 mM HCO2NH4(pH 3.0)/CH3CN = 10/90, B: 100 mM HCO2NH4(pH 3.0)/CH3CN = 70/30

Frow rate

0.36 mL/min

Column temp.

40°C

Injection volume

1.0 µL (5.0 µg/mL)

View detail

LC

Samples

Fucose , Xylose , GalNAc , Mannose , Glucose , GluNAc , Galactose , Neu5Ac , Glucuronic acid

Applications

Glycan-constituting monosaccharides

Column

ULTRON AF-HILIC-CD

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

A: 200 mM CH3CO2NH4(pH 6.8)/CH3CN = 10/90 (for peak 1 to 7), B: 200 mM CH3CO2NH4(pH 6.8)/CH3CN = 18/82 (for peak 8 and 9)

Frow rate

0.26 mL/min

Column temp.

45°C

Injection volume

1.0 µL

View detail

LC

Samples

1-Methylpyrazole , Fomepizole , Pyrazole , 1H-1,2,3-Triazole , Pyrazoline , Imidazole ,

Applications

Analysis of heterocyclic compounds

Column

ULTRON AF-HILIC-DA

Column Size

100 mm L × 4.6 mm I.D.

Mobile phase

20mM HCO2NH4 (pH3.2) /CH3CN = 10/90

Frow rate

0.50 mL/min

Column temp.

30°C

Injection volume

4.0 µL

Diluent

mobile phase

View detail

LC

Samples

Maleic acid , Pyruvic acid , Ascorbic acid , Gluconic acid , Adipic acid , Fumaric acid , Tartaric acid , Malic acid , Citric acid

Applications

Analysis of organic acid

Column

ULTRON AF-HILIC-CD (PLSS)

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

100mM CH3CO2NH4 (pH6.8) /CH3CN = 25/75

Frow rate

0.20 mL/min

Column temp.

40°C

Injection volume

2.0 µL

Diluent

mobile phase

View detail

LC

Samples

Allantoin , Xanthine , Hypoxanthine , Uric acid

Applications

Analysis of Uric acid metabolite

Column

ULTRON AF-HILIC-CD

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

10mM CH3CO2NH4 (pH4.7) /CH3CN = 10/90

Frow rate

0.35 mL/min

Column temp.

30°C

Injection volume

1.0 µL

Diluent

Dissolved samples in 0.1% NaOH aq and add acetonitrile into ratio to 50%

View detail

LC

Samples

Turanose , Palatinose , Maltulose , Maltose , Lactose , Trehalose

Applications

Analysis of disaccharides with different glycosidic linkages

Column

ULTRON AF-HILIC-CD

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

100mM CH3CO2NH4 (pH6.8) /CH3CN = 10/90

Frow rate

0.45 mL/min

Column temp.

40°C

Injection volume

1.0 µL

Diluent

H2O /CH3CN = 50/50

View detail

LC

Samples

Val-Tyr-Val , Leucine Enkephalin , Methionine Enkephalin , Gly-Tyr

Applications

Analysis of peptide standards

Column

ULTRON AF-HILIC-CD

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

A: 10mM HCO2NH4 (pH3.0) /CH3CN = 10/90, B: 10mM HCO2NH4 (pH3.0) /CH3CN = 70/30

Frow rate

0.26 mL/min: 67% A/ 33% B (70.0% CH3CN)

Column temp.

40°C

Injection volume

2.0 µL

Diluent

H2O /CH3CN = 50/50

View detail

LC

Samples

Glycopyrronium bromide

Applications

Analysis of Glycopyrronium bromide

Column

ULTRON ES-OVM

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM KH2PO4 + 20mM K2HPO4 (pH 5.5)/C2H5OH = 95/5

Frow rate

1.0 mL/min

Column temp.

25°C

Injection volume

2.0 µL

View detail

LC

Samples

Glycopyrrolate , Glycopyrrolate erythro isomer

Applications

Analysis of Glycopyrrolate

Column

ULTRON ES-CD

Column Size

250 mm L × 4.6 mm I.D.

Mobile phase

23.3 mM NaH2PO4(pH 6.5)/CH3OH/CH3CN = 40/50/10

Frow rate

1.0 mL/min

Column temp.

30°C

Injection volume

10.0 µL

Diluent

mobile phase

View detail