GC

Samples

n-Hexane , Methyl Alcohol , Acetone , Isopropyl Alcohol , Ethyl Acetate , Methyl Ethyl Ketone , Benzene , Trichloroethylene , Isobutyl Alcohol , Isobutyl Acetate , Toluene , n-Butyl Acetate , Isoamyl Alcohol , Ethylbenzene , m-Xylene , o-Xylene , n-Propylbenzene , Cyclohexanone

Applications

Organic solvent in the air (ppm level)

Column

SBS-100 10% Shimalite TPA 60-80

Column Size

3.1m×3.2mm

Column temp.

110°C

Carrier gas

N2,30ml/min

Injection port temp.

200°C

Detector temp.

200°C(FID)

View detail

GC

Samples

Acetone , Isopropyl Alcohol , n-Hexane , Ethyl Acetate , Chloroform , Carbon Tetrachloride , n-Butyl Alcohol , Methyl Isobutyl Ketone , Isobutyl Acetate , Toluene , n-Butyl Acetate , Ethylbenzene , m-Xylene , o-Xylene , Cyclohexanone , Butyl Cellosolve , 1,1,2,2-Tetrachloroethane , o-Dichlorobenzene

Applications

Organic solvent in work environment (2)

Column

SBS-200 20% Shimalite W 100-120 (AW-DMCS)

Column Size

3.1m×3.2mm

Column temp.

100°C

Carrier gas

N2,50ml/min

Injection port temp.

240°C

Detector temp.

240°C(FID)

View detail

GC

Samples

Acetone , Isopropyl Alcohol , n-Hexane , Ethyl Acetate , Chloroform , Carbon Tetrachloride , n-Butyl Alcohol , Methyl Isobutyl Ketone , Isobutyl Acetate , Toluene , n-Butyl Acetate , Ethylbenzene , m-Xylene , o-Xylene , Cyclohexanone , Butyl Cellosolve , 1,1,2,2-Tetrachloroethane , o-Dichlorobenzene

Applications

Organic solvents of the atmosphere (ppm level)

Column

SBS-200 20% Shimalite W 100-120 (AW-DMCS)

Column Size

3.1m×3.2mm

Column temp.

100°C

Carrier gas

N2,50ml/min

Injection port temp.

240°C

Detector temp.

240°C(FID)

View detail

GC

Samples

n-Pentane , n-Hexane , n-Heptane , n-Octane , Acrolein , Carbon Tetrachloride , Benzene , Acrylonitrile , Acetonitrile , Perchloroethylene , Toluene , Ethylbenzene , m-Xylene , o-Xylene , n-Dodecane , Styrene monomer , n-Tridecane , p-Xylene

Applications

Organic solvent in work environment (1)

Column

Thermon-1000 25% Shimalite 80-100 (AW-DMCS)

Column Size

3.1m×3.2mm

Column temp.

130°C

Carrier gas

N2,40ml/min

Injection port temp.

240°C

Detector temp.

240°C(FID)

View detail

GC

Samples

Ethanol , Acetonitrile , Isopropanol , n-Hexane

Applications

Lower alcohol in water and Hydrocarbon

Column

Thermon-1000 5% Sunpak-A

Column Size

2.1m×3.2mm

Column temp.

180°C

Carrier gas

N2,50ml/min

Injection port temp.

250°C

Detector temp.

230°C(FID)

View detail

GC

Samples

Pynacol , Butanediol(1,4) , Pentanediol(1,5) , Hexanediol(1,6) , Heptanediol(1,7) , Octanediol(1,8) , Nonanediol(1,9) , Decanediol(1,10)

Applications

Diols (standard mixed sample)

Column

Thermon-3000 10% Chromosorb W 80-100 (AW-DMCS)

Column Size

3.1m×3.2mm

Column temp.

228°C

Carrier gas

N2,60ml/min

Injection port temp.

270°C

Detector temp.

260°C(FID)

View detail

GC

Samples

n-Pentane , n-Hexane , Benzene , iso-Octane , Toluene , Ethylbenzene , m-Xylene , o-Xylene , p-Xylene

Applications

Premium gasoline

Column

ULBON HR-1

Column Size

50m×0.25mm(0.5μm)

Column temp.

60°C→220°C(4°C/min)

Carrier gas

He,0.75ml/min

Detector temp.

250°C(FID)

Injection volume

0.5μl

View detail

GC

Samples

n-Pentane , n-Hexane , Benzene , iso-Octane , Toluene , Ethylbenzene , m-Xylene , o-Xylene , p-Xylene

Applications

Regular gasoline

Column

ULBON HR-1

Column Size

50m×0.25mm(0.5μm)

Column temp.

60°C→220°C(4°C/min)

Carrier gas

He,0.75ml/min

Detector temp.

250°C(FID)

Injection volume

0.5μl

View detail

GC

Samples

Solvents (4)

Applications

Solvents (4)

Column

ULBON HR-1701

Column Size

50m×0.25mm(0.5μm)

Column temp.

60°C→180°C(4°C/min)

Carrier gas

He,1.4ml/min

Detector temp.

200°C(FID)

Injection volume

1μl

View detail

GC

Samples

n-Hexane , Ethyl Ether , Acetone , Methyl Acetate , trans-1,2-Dichloroethylene , Methanol , Isopropyl Acetate , Isopropanol , Dichloromethane , n-Propyl Acetate , cis-1,2-Dichloroethylene , Methyl Isobutyl Ketone , Chloroform , Toluene , 1,4-Dioxane , Isobutanol , Isoamyl Acetate , Ethylbenzene , p-Xylene , m-Xylene , Methyl Cellosolve , o-Xylene , Ethyl Cellosolve , Styrene , Cellosolve Acetate , N,N-Dimethylformamide , 4-Methylcyclohexanone , Butyl Cellosolve , cis-4-Methylcyclohexanol , m-Dichlorobenzene , p-Dichlorobenzene , trans-4-Methylcyclohexanol , o-Dichlorobenzene , o-Cresol , p-Cresol , m-Cresol

Applications

Solvents (6)

Column

ULBON HR-20M

Column Size

50m×0.25mm(0.5μm)

Column temp.

60°C→240°C(3°C/min)

Carrier gas

He,1.3ml/min

Detector temp.

250°C(FID)

Injection volume

1μl

View detail

GC

Samples

Methanol , Acetone , Dichloromethane , trans-1,2-Dichloroethylene , n-Hexane , Ethyl Acetate , Tetrahydrofuran , 1,1,1-Trichloroethane , Carbon Tetrachloride , Trichloroethylene , Methyl Isobutyl Ketone , Toluene , Methyl Butyl Ketone , Tetrachloroethylene , Chlorobenzene , Ethylbenzene , p-Xylene , Styrene , 1,1,2,2-Tetrachloroethane , 2-Methylcyclohexanone , 4-Methylcyclohexanone , m-Dichlorobenzene , p-Dichlorobenzene , o-Cresol , p-Cresol

Applications

The work environment (1)

Column

ULBON HR-52

Column Size

30m×0.53mm(5μm)

Column temp.

60°C→130°C(3°C/min)

Carrier gas

He,8.0ml/min

Detector temp.

150°C(FID)

Injection volume

1ml

View detail

GC

Samples

Methanol , Ethanol , Acetone , n-Propanol , n-Hexane , Ethyl Acetate , Chloroform , Benzene , MIBK , Toluene , Isobutyl Acetate , n-Butyl Acetate , Ethylbenzene , m-Xylene , o-Xylene , Cellosolve Acetate

Applications

Solvents (1)

Column

ULBON HR-52

Column Size

25m×0.32mm(0.5μm)

Column temp.

40°C→90°C(2°C/min)

Carrier gas

He,0.83ml/min

Detector temp.

200°C(FID)

Injection volume

1μl

View detail

GC

Samples

Methanol , Acetone , Dichloromethane , trans-1,2-Dichloroethylene , n-Hexane , Ethyl Acetate , Tetrahydrofuran , 1,1,1-Trichloroethane , Carbon Tetrachloride , Trichloroethylene , 1,4-Dioxane , Methyl Isobutyl Ketone , Toluene , Methyl n-Butyl Ketone , n-Butyl Acetate , Tetrachloroethylene , Chlorobenzene , Ethylbenzene , p-Xylene , Styrene , o-Xylene , Butyl Cellosolve , 1,1,2,2-Tetrachloroethane , 3-Methylcyclohexanol(cis, trans) , 2-Methylcyclohexanone , 4-Methylcyclohexanone , m-Dichlorobenzene , p-Dichlorobenzene , o-Dichlorobenzene , o-Cresol , p-Cresol

Applications

Solvents (3)

Column

ULBON HR-52

Column Size

50m×0.25mm(0.5μm)

Column temp.

60°C→130°C(3°C/min)

Carrier gas

He,1.2ml/min

Detector temp.

200°C(FID)

Injection volume

1μl

View detail

GC

Samples

n-Hexane, Benzene , n-Octane , Toluene , n-Nonane , Ethylbenzene , p-Xylene , m-Xylene , o-Xylene , Isopropylbenzene , Styrene , n-Propylbenzene , p-Ethyltoluene , m-Ethyltoluene , o-Ethyltoluene , 1,3,5-Trimethylbenzene , 1,2,4-Trimethylbenzene , 1,2,3-Trimethylbenzene , 4-n-Propyltoluene , 3-n-Propyltoluene , 2-n-Propyltoluene , 1,2,3,5-Tetramethylbenzene , 1,2,4,5-Tetramethylbenzene , 1,2,3,4-Tetramethylbenzene

Applications

Alkyl benzene isomer

Column

ULBON Xylene Master

Column Size

50m×0.32mm

Column temp.

70°C→120°C(2°C/min)

Carrier gas

He,1.4ml/min

Detector temp.

200°C(FID)

Injection volume

1μl

View detail

GC

Samples

Methyl mercuric chloride , Ethyl mercuric chloride

Applications

Measurement of alkyl mercury compounds (each 100 ppb in n-hexane) using Shinwasorb

Column

Thermon-HG 5% Shinwasorb-U 60/80

Column Size

0.5 m x 3.0 mm I.D. Glass

Column temp.

160℃

Carrier gas

50 mL/min N₂

Injection port temp.

250℃

Detector temp.

250℃

Detector

ECD

Injection volume

1.0 μL

View detail

GC

Samples

Ethylbenzene , p-Xylene , m-Xylene , o-Xylene

Applications

Measurement of xylene isomers using Shinwasorb

Column

Shinchrom F51+Bentone 34 3+2% Shinwasorb-U 60/80

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

80℃

Carrier gas

40 mL/min N₂

Injection port temp.

240℃

Detector temp.

240℃

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

Mixture of 13 organic solvents

Applications

Measurement of organic solvents using Shinwasorb -1-

Column

PEG1500 12.5% Shinwasorb-U 40/60

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

70℃

Carrier gas

40 mL/min N₂

Injection port temp.

200℃

Detector temp.

200℃

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

Mixture of 22 organic solvents

Applications

Measurement of organic solvents using Shinwasorb -2-

Column

PEG1500 12.5% Shinwasorb-U 40/60

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

60～120℃ (4℃/min)

Carrier gas

40 mL/min N₂

Injection port temp.

200℃

Detector temp.

200℃

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

Fragrance

Applications

Measurements of fragrance using Shinwasorb

Column

Thermon-3000 5% Shinwasorb-S 80/100

Column Size

2.1 m x 3.2 mm I.D. Glass

Column temp.

80～260℃（6℃/min)

Carrier gas

50 mL/min N₂

Injection port temp.

280℃

Detector temp.

280℃

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

200 ppm in hexane

Applications

Measurements of eucalyptus oil using Shinwasorb

Column

Thermon-3000 5% Shinwasorb-S 80/100

Column Size

5.1 m x 3.2 mm I.D. Glass

Column temp.

120℃ & 130℃

Carrier gas

40 mL/min N₂

Injection port temp.

200℃

Detector temp.

200℃

Detector

FID

Injection volume

2.0 μL

View detail

GC

Samples

Isopropyl iodide , Methylcyclohexane , o-xylene

Applications

Analysis of hydroxypropylcellulose (JP)

Column

ULBON HR-1

Column Size

0.53 mm I.D. x 30 m df = 3.0 µm

Column temp.

40℃ (3 min)～10℃/min～100℃～50℃/min～250℃ (3 min)

Carrier gas

52 cm/sec He

Injection port temp.

180°C

Detector temp.

280°C

Detector

FID

Injection volume

2.0 μL Split rate: 1:50

View detail

GC

Samples

Cyclohexane , N,N-dimethylaniline , Naphthalene ,

Applications

Analysis of ampicillin hydrate using Shinwasorb

Column

Silicone OV-17 1.5% Shinwasorb-S 60/80

Column Size

2.1 m x 2.6 mm I.D. Glass

Column temp.

105℃

Carrier gas

20 mL/min He（adjust so that the retention time of N,N-dimethylaniline is about 5 minutes.)

Injection port temp.

200°C

Detector temp.

200°C

Detector

FID

Injection volume

1.0 μL

View detail

GC

Samples

Cyclohexane , Ethyl acetate , 2-propanol ,

Applications

Analysis of lenampicillin hydrochloride using Shinwasorb

Column

Quadrol 5% Shinwasorb-S 60/80

Column Size

3.1 m x 3.2 mm I.D. Glass

Column temp.

100℃

Carrier gas

70 mL/min N₂ (Adjust so that the retention time of cyclohexane is about 1 minute.)

Injection port temp.

160°C

Detector temp.

160°C

Detector

FID

Injection volume

4.0 μL

View detail

GC

Samples

Cyclohexane , Dicyclohexyl phthalate , Etofenprox

Applications

Analysis of etofenprox using Shinwasorb

Column

Silicone OV-225 2.5% Shinwasorb-U 60/80

Column Size

1.1m x 3.2 mm I.D. Glass

Column temp.

240℃

Carrier gas

37 mL/min N₂ (Adjust so that the retention time of dicyclohexyl phthalate is about 8 minutes.)

Injection port temp.

250°C

Detector temp.

250°C

Detector

FID

Injection volume

3.0 μL

View detail

GC

Samples

Etofenprox in Cyclohexane

Applications

Analysis of etofenprox using Shinwasorb -2- ～Purity (3) Related substances～

Column

Silicone OV-225 2.5% Shinwasorb-U 60/80

Column Size

1.1m x 3.2 mm I.D. Glass

Column temp.

240℃

Carrier gas

37 mL/min N₂

Injection port temp.

250°C

Detector temp.

250°C

Detector

FID

Injection volume

3.0 μL

View detail

GC

Samples

Diethyl ether , n-Hexane , Methanol , Methyl acetate , 2-Propanol , Ethyl acetate , Tetrahydrofuran , 2-Butanol , iso-Butanol , Toluene , n-Butyl acetate , Methyl n-butyl ketone , iso-Amyl alcohol , Ethylbenzene , m-Xylene , p-Xylene , o-Xylene , Styrene monomer ,

Applications

Measurement of organic solvents using SBS-120

Column

SBS-120 12% Shincarbon-A2 80/100

Column Size

3.1 m x 3.2 mm I.D. Glass

Column temp.

90℃

Carrier gas

40 mL/min N₂

Injection port temp.

230℃

Detector temp.

230℃

Detector

FID

Injection volume

1.0 μL

View detail

LC

Samples

1,1'-Bi-2-naphthol

Applications

1,1'-Bi-2-naphthol

Column

ULTRON ES-PhCD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

n-Hexane/Dichloromethane/CH3OH = 75/25/5

Frow rate

1.2 mL/min

Column temp.

25°C

View detail

LC

Samples

trans-Stilbene oxide

Applications

Analysis in normal phase mobile phase

Column

ULTRON ES-PhCD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

n-Hexane/CH3OH = 99.9/0.1

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

N-(3,5-Dinitrobenzoyl)-α-Methylbenzylamine

Applications

Analysis in normal phase mobile phase

Column

ULTRON ES-PhCD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

n-Hexane/C2H5OH = 85/15

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Flavanone

Applications

Analysis in normal phase mobile phase

Column

ULTRON ES-PhCD

Column Size

150 mm L × 6.0 mm I.D.

Mobile phase

n-Hexane/C2H5OH = 99/1

Frow rate

1.0 mL/min

Column temp.

25°C

View detail

LC

Samples

Citric acid , Tartaric acid , Malic acid , Malonic acid , Succinic acid , Glycolic acid , Formic acid , Lactic acid , Acetic acid , Fumaric acid , Adipic acid , Pyroglutamic acid , Propionic acid , Acrylic acid , Pivalic acid , Methacrylic acid , Crotonic acid

Applications

Elution position of the aliphatic organic acid

Column

ULTRON PS-80H

Column Size

300 mm L × 8.0 mm I.D. + 300 mm L × 8.0 mm I.D.

Mobile phase

HClO4aq. (pH 2.1)

Frow rate

1.0 mL/min

Column temp.

60°C

View detail

LC

Samples

Sucrose , Lactose , Glucose , Xylose , Galactose , Fructose , Inositol

Applications

Sugar and alditol

Column

ULTRON PS-80P

Column Size

300 mm L × 8.0 mm I.D.

Mobile phase

H2O

Frow rate

1.0 mL/min

Column temp.

80°C

Pressure

2.0 MPa

View detail

LC

Samples

Pyridoxal , Pyridoxine , Pyridoxamine

Applications

The water-soluble vitamin (2)

Column

STR ODS-II

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

100 mM Phosphoric acid buffer(pH 2.1) + 50 mM Hexane sodium sulphonate/CH3CN = 9/1

Frow rate

1.0 mL/min

Column temp.

45°C

View detail

LC

Samples

Nicotinic acid , Nicotinic acid amide , Calcium pantothenate , Pyridoxine hydrochloride , Riboflavin phosphate , Thiamine , Folic acid , Biotin , Riboflavin

Applications

The water-soluble vitamin

Column

ULTRON VX-ODS

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

20 mM H3PO4/5 mM Sodium 1-hexanesulfonate = 91/9

Frow rate

1.0 mL/min

Column temp.

45°C

View detail

LC

Samples

Estrone , Estradiol , Estriol

Applications

Female sex hormone

Column

ULTRON VX-SIL

Column Size

150 mm L × 4.6 mm I.D.

Mobile phase

n-Hexane/C2H5OH = 90/10

Frow rate

1.0 mL/min

Column temp.

ambient

View detail

LC

Samples

Xylose , Fructose , Glucose , Mannitol , Xylobiose , Sucrose , Lactulose , Lactose , Trehalose , Xylotriose , 1-Kestose(GF2) , Raffinose , Nystose(GF3) ,

Applications

Analysis of monosaccharides, disaccharides, and oligosaccharides

Column

ULTRON AF-HILIC-CD

Column Size

100 mm L × 2.0 mm I.D.

Mobile phase

A: H2O /CH3CN = 10/90, B: H2O /CH3CN = 70/30

Frow rate

0.26 mL/min

Column temp.

40°C

Injection volume

1.0 µL

Diluent

H2O /CH3CN = 50/50

View detail

LC

Samples

Xylose , Fructose , Glucose , Mannitol , Xylobiose , Sucrose , Lactulose , Lactose , Trehalose , Xylotriose , 1-Kestose(GF2) , Raffinose , Nystose(GF3) ,

Applications

Analysis of monosaccharides, disaccharides, and oligosaccharides

Column

ULTRON AF-HILIC-CD

Column Size

100 mm L × 2.0 mm I.D.

Mobile phase

A: 20mM CH3CO2NH4 (pH6.8) /CH3CN = 10/90, B: 20mM CH3CO2NH4 (pH6.8) /CH3CN = 70/30

Frow rate

0.26 mL/min

Column temp.

40°C

Injection volume

2.5 µL

Diluent

H2O /CH3CN = 50/50

View detail

LC

Samples

Erythritol , Xylitol , Fructose , Glucose , Sorbitol , Sucrose , Inositol , Maltose , Maltitol , Lactose , Lactitol

Applications

Analysis of saccharides and sweeteners

Column

ULTRON AF-HILIC-CD

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

A: 100mM CH3CO2NH4 (pH6.8) /CH3CN = 10/90, B: 100mM CH3CO2NH4 (pH6.8) /CH3CN = 70/30

Frow rate

0.32 mL/min

Column temp.

40°C

Injection volume

1.0 µL

Diluent

H2O /CH3CN = 50/50

View detail

LC

Samples

Maleic acid , Pyruvic acid , Ascorbic acid , Gluconic acid , Adipic acid , Fumaric acid , Tartaric acid , Malic acid , Citric acid

Applications

Analysis of organic acid

Column

ULTRON AF-HILIC-CD (PLSS)

Column Size

150 mm L × 2.0 mm I.D.

Mobile phase

100mM CH3CO2NH4 (pH6.8) /CH3CN = 25/75

Frow rate

0.20 mL/min

Column temp.

40°C

Injection volume

2.0 µL

Diluent

mobile phase

View detail

LC

Samples

myo-inositol , 1-propanol

Applications

Analysis of Inositol ～conform to Japanese Pharmaceutical Excipients 2018～

Column

ULTRON PS-80N

Column Size

300 mm L × 8.0 mm I.D.

Mobile phase

H2O

Frow rate

0.87 mL/min

Column temp.

65°C

Injection volume

10 µL

Diluent

H2O

View detail