Shinwa Chemical Industries Ltd.
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Shinwa Chemical Industries
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"ALA" Filtered 33 Item.

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GC

Samples
Methane , Ethane , Ethylene , Propane , iso-Butane , Propylene , n-Butane
Applications
Ethane and ethylene in the exhaust gas
Column
Squalane 1% Activated Alumina 60-80
Column Size
1.1m×3.2mm
Column temp.
40°C
Carrier gas
N2,30ml/min
Injection port temp.
40°C
Detector temp.
40°C(FID)

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GC

Samples
Diethyl Phthalate , Di-iso-Butyl Phthalate , Di-n-Butyl Phthalate , Di-n-Amyl Phthalate , Diheptyl Phthalate , Dioctyl Phthalate
Applications
Phthalic acid ester (2) (200ppm)
Column
Thermon-3000 2% Chromosorb W 80-100 (AW-DMCS)
Column Size
2.1m×3.2mm
Column temp.
215°C
Carrier gas
N2,65ml/min
Injection port temp.
260°C
Detector temp.
260°C(FID)

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GC

Samples
Dimethyl Phthalate , Diethyl Phthalate , Diallyl Phthalate , Di-iso-Butyl Phthalate , Di-n-Butyl Phthalate , Di-n-Amyl Phthalate , Di-2-Ethylhexyl Phthalate , Di-n-Octyl Phthalate
Applications
Phthalic acid ester (1)
Column
ULBON HR-1
Column Size
25m×0.25mm(0.25μm)
Column temp.
180°C→300°C(6°C/min)
Carrier gas
He,0.98ml/min
Detector temp.
320°C(FID)
Injection volume
0.5μl

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GC

Samples
n-Butyl Formate , n-Butyl Acetate , n-Butyl Propionate , n-Butyl iso-Butyrate , n-Butyl n-Butyrate , n-Butyl Crotonate , n-Butyl n-Caproate , n-Butyl Lactate , n-Butyl n-Caprate , Di-n-Butyl Oxalate , n-Butyl Benzoate , Di-n-Butyl Malonate , Di-n-Butyl Fumarate , Di-n-Butyl Succinate , Di-n-Butyl Maleate , Di-n-Butyl Adipate , Di-n-Butyl Maleate , Di-n-Butyl Phthalate , Di-n-Butyl Sebacate , Di-n-Butyl Isophthalate , Di-n-Butyl Terephthalate , Tri-n-Butyl Citrate
Applications
Organic acid butyl ester
Column
ULBON HR-20M
Column Size
25m×0.25mm(0.25μm)
Column temp.
80°C→240°C(4°C/min)
Carrier gas
He,1.1ml/min
Detector temp.
250°C(FID)
Injection volume
1.0μm

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GC

Samples
β-Pinene , Limonene , Linalool , Linalyl Acetate , Benzyl Acetate , α-Ionene , Phenethyl Alcohol , Lauryl Alcohol , Eugenol , Diethyl Phthalate , Vanillin , Benzyl Salicylate
Applications
perfume (2)
Column
ULBON HR-Thermon-600T
Column Size
50m×0.25mm
Column temp.
70°C→230°C(4°C/min)
Carrier gas
He,1.1ml/min
Detector temp.
250°C(FID)

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GC

Samples
Fragrance
Applications
Measurements of fragrance using Shinwasorb
Column
Thermon-3000 5% Shinwasorb-S 80/100
Column Size
2.1 m x 3.2 mm I.D. Glass
Column temp.
80~260℃(6℃/min)
Carrier gas
50 mL/min N₂
Injection port temp.
280℃
Detector temp.
280℃
Detector
FID
Injection volume
1.0 μL

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GC

Samples
Ethyl acetate , di-n-butyl phthalate , Teprenone (mono-cis isomer) , Teprenone (all-trans isomer) , ,
Applications
Analysis of teprenone using Shinwasorb -1-
Column
FFAP 5% Shinwasorb-U 80/100
Column Size
2.1m×3.2mm glass
Column temp.
235°C
Carrier gas
47 mL/min N2
Injection port temp.
270°C
Detector temp.
270°C
Detector
FID
Injection volume
2.0 μL

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GC

Samples
Ethyl acetate , di-n-butyl phthalate , Teprenone (mono-cis isomer) , Teprenone (all-trans isomer) , ,
Applications
Analysis of teprenone using Shinwasorb -2-
Column
FFAP 5% Shinwasorb-U 80/100
Column Size
2.1m×3.2mm glass
Column temp.
235°C
Carrier gas
47 mL/min N2
Injection port temp.
270°C
Detector temp.
270°C
Detector
FID
Injection volume
2.0 µL

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GC

Samples
Deet, diethyl phthalate in ethanol
Applications
Analysis of deet (Pesticide guidelines) ~Purity test (4) Related substances~
Column
ULBON HR-20M
Column Size
0.2 mm I.D. x 25 m df = 0.1 µmm
Column temp.
170℃
Carrier gas
21 cm/sec He (Adjust so that the retention time of deet is about 10 minutes.)
Injection port temp.
230°C
Detector temp.
230°C
Detector
FID
Injection volume
2.0 μL (Split rate: 1:70)

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GC

Samples
2-propanol, ethanol in water
Applications
Analysis of sodium aurothiomalate using Sunpak-H ~Purity test (4) Ethanol~
Column
Sunpak-H 80/100
Column Size
3.1m x 3.2 mm I.D. Glass
Column temp.
145℃
Carrier gas
28 mL/min N2 (Adjust so that the retention time of 2-propanol is about 7 minutes.)
Injection port temp.
230°C
Detector temp.
230°C
Detector
FID
Injection volume
2.0 μL

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GC

Samples
Cyclohexane , Dicyclohexyl phthalate , Etofenprox
Applications
Analysis of etofenprox using Shinwasorb
Column
Silicone OV-225 2.5% Shinwasorb-U 60/80
Column Size
1.1m x 3.2 mm I.D. Glass
Column temp.
240℃
Carrier gas
37 mL/min N₂ (Adjust so that the retention time of dicyclohexyl phthalate is about 8 minutes.)
Injection port temp.
250°C
Detector temp.
250°C
Detector
FID
Injection volume
3.0 μL

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GC

Samples
Acetone , Allethrin , Di(2-ethylhexyl) phthalate
Applications
Analysis of allethrin using Shinwasorb Part 3
Column
Diethyleneglycol Succinate (DEGS) 2.5% Shinwasorb-U 80/100
Column Size
1.1 m x 3.2 mm I.D. Glass
Column temp.
200℃
Carrier gas
36 mL/min N₂ (Adjust so that the retention time of allethrin is about 8 minutes.)
Injection port temp.
230°C
Detector temp.
230°C
Detector
FID
Injection volume
1.0 μL

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GC

Samples
Diazinon, Di-n-butyl phthalate in Acetone
Applications
Analysis of diazinon using Shinwasorb
Column
Silicone OV-11 10% Shinwasorb-U 60/80
Column Size
1.6 m x 3.2 mm I.D. Glass
Column temp.
200℃
Carrier gas
25 mL/min N₂(Adjust so that the retention time of diazinon is about 7 minutes.)
Injection port temp.
230°C
Detector temp.
230°C
Detector
FID
Injection volume
3.0 μL

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GC

Samples
Anhydrous caffeine, Fenitrothion in Acetone
Applications
Analysis of Fenitrothion Emulsifiable Concentrate using Shinwasorb
Column
Silicone OV-210 3% Shinwasorb-S 80/100
Column Size
2.1 m x 3.2 mm I.D. Glass
Column temp.
175℃
Carrier gas
51 mL/min N₂(Adjust so that the retention time of Anhydrous caffeine is about 10 minutes.)
Injection port temp.
230°C
Detector temp.
230°C
Detector
FID
Injection volume
2.0 μL

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LC

Samples
(1S,2R)-1-Methyl cis-1,2,3,6-tetrahydrophthalate
Applications
(1S,2R)-1-Methyl cis-1,2,3,6-tetrahydrophthalate
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4(pH 4.0)/CH3CN = 100/5
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Sucrose , Lactose , Glucose , Galactose , Fructose
Applications
Yoghurt drink
Column
ULTRON PS-80C
Column Size
300 mm L × 8.0 mm I.D.
Mobile phase
H2O
Frow rate
0.5 mL/min
Column temp.
80°C
Pressure
2.0 MPa
Injection volume
10 µL

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LC

Samples
Glucuronic acid , N-Acetylglucosamine , N-Acetylgalactosamine
Applications
Uronic acid, Acetylation amino sugar
Column
ULTRON PS-80H
Column Size
300 mm L × 8.0 mm I.D.
Mobile phase
HClO4aq.(pH 2.1)
Frow rate
1.0 mL/min
Column temp.
60°C
Pressure
2.5 MPa

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LC

Samples
Sucrose , Lactose , Glucose , Xylose , Galactose , Fructose , Inositol
Applications
Sugar and alditol
Column
ULTRON PS-80P
Column Size
300 mm L × 8.0 mm I.D.
Mobile phase
H2O
Frow rate
1.0 mL/min
Column temp.
80°C
Pressure
2.0 MPa

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LC

Samples
Aspartic acid , Glutamic acid , Serine , Glycine , Histidine , Arginine , Threonine , Alanine , Proline , Tyrosine , Valine , Methionine , Cysteine-cysteine , Isoleucine , Leucine , Phenylalanine , Lysine
Applications
Analysis of the PTC amino acid
Column
STR ODS-II
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
A: CH3COONa(pH 6.5)/CH3CN = 93/7, B: CH3CN/H2O = 4/1
Frow rate
1.0 mL/min
Column temp.
40°C

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LC

Samples
Escitalopram oxalate
Applications
Escitalopram oxalate
Column
ES-OVM , ES-OVM-E
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
50 mM KH2PO4 + 0.2 N NaOH(pH 7.0)/CH3CN = 85/15
Frow rate
0.6 mL/min
Column temp.
30°C

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LC

Samples
Nicotinamide , Pyridoxine , Isoascorbic acid , Riboflavin , Nicotinic acid , Ascorbic acid , Biotin , Pantothenic acid , Folic acid , Cyanocobalamin , Thiamine
Applications
Water-soluble vitamins
Column
ULTRON AF-HILIC-CD
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
A: 20 mM CH3CO2NH4(pH 6.8)/CH3CN = 10/90, B: 20 mM CH3CO2NH4(pH 6.8)/CH3CN = 70/30
Frow rate
0.25 mL/min
Column temp.
30°C
Injection volume
1.0 µL

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LC

Samples
(CYS)2 , LYS , ARG , HIS , ASP , GLU , GLN , ASN , GLY , SER , ALA , THR , PRO , TYR , VAL , PHE , MET , TRP , LEU+ILE
Applications
Analysis of underivatized amino acids by LC/MS/MS
Column
ULTRON AF-HILIC-CD (PLSS)
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
A: 100 mM HCO2NH4(pH 3.0)/CH3CN = 10/90, B: 100 mM HCO2NH4(pH 3.0)/CH3CN = 70/30
Frow rate
0.36 mL/min
Column temp.
40°C
Injection volume
1.0 µL (5.0 µg/mL)

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LC

Samples
Fucose , Xylose , GalNAc , Mannose , Glucose , GluNAc , Galactose , Neu5Ac , Glucuronic acid
Applications
Glycan-constituting monosaccharides
Column
ULTRON AF-HILIC-CD
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
A: 200 mM CH3CO2NH4(pH 6.8)/CH3CN = 10/90 (for peak 1 to 7), B: 200 mM CH3CO2NH4(pH 6.8)/CH3CN = 18/82 (for peak 8 and 9)
Frow rate
0.26 mL/min
Column temp.
45°C
Injection volume
1.0 µL

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LC

Samples
L-DOPA , Dopamine , Adrenaline , Noradrenaline
Applications
Analysis of catecholamines
Column
ULTRON AF-HILIC-DA
Column Size
100 mm L × 4.6 mm I.D.
Mobile phase
20mM CH3CO2NH4 (pH4.7) /CH3CN = 10/90
Frow rate
0.50 mL/min
Column temp.
30°C
Injection volume
4.0 µL
Diluent
Mobile phase

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LC

Samples
Turanose , Palatinose , Maltulose , Maltose , Lactose , Trehalose
Applications
Analysis of disaccharides with different glycosidic linkages
Column
ULTRON AF-HILIC-CD
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
100mM CH3CO2NH4 (pH6.8) /CH3CN = 10/90
Frow rate
0.45 mL/min
Column temp.
40°C
Injection volume
1.0 µL
Diluent
H2O /CH3CN = 50/50

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LC

Samples
Val-Tyr-Val , Leucine Enkephalin , Methionine Enkephalin , Gly-Tyr
Applications
Analysis of peptide standards
Column
ULTRON AF-HILIC-CD
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
A: 10mM HCO2NH4 (pH3.0) /CH3CN = 10/90, B: 10mM HCO2NH4 (pH3.0) /CH3CN = 70/30
Frow rate
0.26 mL/min: 67% A/ 33% B (70.0% CH3CN)
Column temp.
40°C
Injection volume
2.0 µL
Diluent
H2O /CH3CN = 50/50

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LC

Samples
Tadalafil
Applications
Analyses of tadalafil in ULTRON ES-OVM series.(Faster analyses with 3µm particles)
Column
ES-OVM
Column Size
(1)150 mm L × 4.6 mm I.D. (2)100 mm L × 3.0 mm I.D.
Mobile phase
20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
(1)2.0 µL (2)0.5 µL
Diluent
methanol

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LC

Samples
Tadalafil
Applications
Analyses of tadalafil in ULTRON ES-OVM series.(Greater analytical performance with 3µm particles)
Column
ES-OVM
Column Size
(1)150 mm L × 4.6 mm I.D. (2)100 mm L × 3.0 mm I.D.
Mobile phase
20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15
Frow rate
(1)1.0 mL/min (2)0.28 mL/min
Column temp.
25°C
Injection volume
(1)2.0 µL (2)0.5 µL
Diluent
methanol

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LC

Samples
escitalopram oxalate
Applications
Analyses of escitalopram oxalate in ULTRON ES-OVM series.(Faster analyses with 3µm particles)
Column
ES-OVM
Column Size
(1)150 mm L × 4.6 mm I.D. (2)100 mm L × 3.0 mm I.D.
Mobile phase
50 mM KH2PO4 + 0.2 N NaOH(pH 7.0)/CH3CN = 85/15
Frow rate
0.6 mL/min
Column temp.
30°C
Injection volume
(1)15.0 µL (2)0.5 µL
Diluent
Mobile phase

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LC

Samples
escitalopram oxalate
Applications
Analysis of escitalopram oxalate
Column
ES-OVM
Column Size
100 mm L × 3.0 mm I.D.
Mobile phase
50 mM KH2PO4 + 0.2 N NaOH(pH 7.0)/CH3CN = 85/15
Frow rate
0.6 mL/min
Column temp.
30°C
Injection volume
0.5 µL
Diluent
Mobile phase

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LC

Samples
Tadalafil
Applications
Analysis of tadalafil
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
2.0 µL
Diluent
methanol

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LC

Samples
Tadalafil
Applications
Analysis of tadalafil
Column
ES-OVM
Column Size
100 mm L × 3.0 mm I.D.
Mobile phase
20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
0.5 µL
Diluent
methanol

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LC

Samples
Tadalafil
Applications
Analysis of tadalafil
Column
ES-OVM
Column Size
100 mm L × 3.0 mm I.D.
Mobile phase
20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15
Frow rate
0.28 mL/min
Column temp.
25°C
Injection volume
0.5 µL
Diluent
methanol

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