Shinwa Chemical Industries Ltd.
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Shinwa Chemical Industries
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"Amine" Filtered 58 Item.

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GC

Samples
Trimethylamine , Dimethylamine , Monomethylamine
Applications
Mono-, di-, trimethylamine
Column
Diglycerol+TEP+KOH(15%+15%+2%) Chromosorb W 80-100 (AW-DMIS)
Column Size
3.1m×3.2mm
Column temp.
70°C
Carrier gas
N2,60ml/min
Injection port temp.
230°C
Detector temp.
230°C(FID)

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GC

Samples
Mono Ethanolamine , Diethanolamine , Triethanolamine
Applications
Tri-, di-, monoethanolamine in water
Column
TENAX TA 60-80
Column Size
1.1m×3.2mm
Column temp.
160°C→270°C(10°C/min)
Carrier gas
N2,40ml/min
Injection port temp.
290°C
Detector temp.
290°C(FID)

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GC

Samples
TETA(Triethylene Tetramine) , TEPA(Tetraethylene Pentamine)
Applications
TETA and TEPA
Column
Thermon-1000+KOH(10%+3%) Chromosorb W 80-100 (AW-DMCS)
Column Size
2.1m×3.2mm
Column temp.
250°C
Carrier gas
N2,55ml/min
Injection port temp.
280°C
Detector temp.
280°C(FID)

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GC

Samples
o-Phenylenediamine , p-Phenylenediamine , m-Phenylenediamine
Applications
Phenylenediamine
Column
Thermon-1000+KOH(10%+3%) Chromosorb W 80-100 (AW-DMCS)
Column Size
2.1m×3.2mm
Column temp.
250°C
Carrier gas
N2,60ml/min
Injection port temp.
280°C
Detector temp.
280°C(FID)

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GC

Samples
Diphenhydramine
Applications
Diphenhydramine
Column
Thermon-3000 5% Chromosorb W 80-100 (AW-DMCS)
Column Size
1.1m×3.2mm
Column temp.
200°C
Carrier gas
N2,80ml/min
Injection port temp.
260°C
Detector temp.
260°C(FID)

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GC

Samples
Monomethylamine , Dimethylamine , Trimethylamine
Applications
Tri-, di-, monomethylamine in Nitrogen
Column
Thermon-3000+KOH(5%+1%) Sunpak-A
Column Size
2.1m×3.2mm
Column temp.
150°C
Carrier gas
N2,50ml/min
Injection port temp.
240°C
Detector temp.
240°C(FID)

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GC

Samples
Methylamine , Dimethylamine , Trimethylamine
Applications
Tri-, di-, monomethylamine in water
Column
Thermon-3000+KOH(5%+1%) Sunpak-A
Column Size
2.1m×3.2mm
Column temp.
140°C
Carrier gas
N2,50ml/min
Injection port temp.
250°C
Detector temp.
230°C(FID)

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GC

Samples
Methanol , Acetaldehyde , Ethanol , Trimethylamine
Applications
Methanol Ethanol Acetaldehyde Trimethylamine in water
Column
Thermon-3000+KOH(5%+1%) Sunpak-A
Column Size
2.1m×3.2mm
Column temp.
120°C
Carrier gas
N2,50ml/min(headspace)
Injection port temp.
220°C
Detector temp.
220°C(FID)

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GC

Samples
Monomethylamine , Dimethylamine , Trimethylamine
Applications
Tri-, di-, monomethylamine in water
Column
Thermon-3000+KOH(5%+1%) Sunpak-A
Column Size
2.1m×3.2mm
Column temp.
140°C
Carrier gas
N2,50ml/min
Injection port temp.
260°C
Detector temp.
260°C(FID)

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GC

Samples
o-Ethoxybenzamide , Phenacetin , Caffeine , Aminopyrine , Chlorpheniramine Maleate
Applications
Medicine
Column
ULBON HR-1
Column Size
15m×0.53mm(1.0μm)
Column temp.
180°C
Carrier gas
He,7.2ml/min
Detector temp.
250°C(FID)
Injection volume
0.5μl

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GC

Samples
n-Octylamine , n-Decylamine , Laurylamine , n-Tetradecylamine , Cetylamine , Stearylamine
Applications
Aliphatic amine
Column
ULBON HR-52
Column Size
25m×0.25mm(0.25μm)
Column temp.
150°C→230°C(4°C/min)
Carrier gas
He,0.48ml/min
Detector temp.
250°C(FID)
Injection volume
1.5μl

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GC

Samples
Trimethylamine , Dimethylamine , Methylamine
Applications
Analysis of methylamines using Shinwasorb
Column
Diglycerol+TEP+KOH 7.5+7.5+1% Shinwasorb-S 60/80
Column Size
3.1 m x 3.2 mm I.D. Glass
Column temp.
70℃
Carrier gas
50 mL/min N₂
Injection port temp.
220℃
Detector temp.
220℃
Detector
FID
Injection volume
1.0 μL

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GC

Samples
homatropine hydrobromide , scopolamine
Applications
Analysis of opium alkaloid scopolamine using Shinwasorb
Column
Silicone OV-17 1% Shinwasorb-S 60/80
Column Size
1.6m×3.2mm glass
Column temp.
210°C
Carrier gas
45 mL/min N2
Injection port temp.
250°C
Detector temp.
250°C
Detector
FID
Injection volume
2.0 μL

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GC

Samples
Ammonia and Mono, Di, Tri-Methylamine in Water ,
Applications
Ammonia and Mono, Di, Tri-Methylamine in Water
Column
Thermon-3000 + KOH 2+2% Sunpak-N 60/100 mesh
Column Size
2.1 m x 3.2 mm I.D. Glass
Column temp.
120℃
Carrier gas
50 mL/min He
Injection port temp.
250°C
Detector temp.
250°C
Detector
TCD
Injection volume
1.0 μL

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LC

Samples
Alimemazine
Applications
Antihistaminic drug
Column
ES-CD
Column Size
150 mm L × 6.0 mm I.D.
Mobile phase
20 mM KH2PO4(pH 5.0)/CH3CN = 70/30
Frow rate
1.2 mL/min
Column temp.
25°C

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LC

Samples
Trimipramine
Applications
Trimipramine
Column
ES-CD
Column Size
150 mm L × 6.0 mm I.D.
Mobile phase
20 mM KH2PO4(pH 4.6)/CH3CN = 75/25
Frow rate
1.2 mL/min
Column temp.
25°C

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LC

Samples
Chlorpheniramine maleate
Applications
Chlorpheniramine maleate
Column
ES-CD
Column Size
150 mm L × 6.0 mm I.D.
Mobile phase
20 mM KH2PO4(pH 4.6)/CH3CN = 83/17
Frow rate
1.0 mL/min
Column temp.
15°C

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LC

Samples
1,2-Diphenylethylamine
Applications
1,2-Diphenylethylamine
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4(pH 5.5)
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Prenylamine
Applications
Calcium rivalry medicine
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4(pH 5.0)/CH3CN = 100/15
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Trimipramine maleate
Applications
Analysis of the antidepressive drug
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4(pH 3.0)/C2H5OH = 100/30
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Profenamine
Applications
Antiparkinsonic agent
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4(pH 4.6)/C2H5OH = 100/25
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Alimemazine
Applications
Antihistaminic drug
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4(pH 4.6)/C2H5OH = 100/25
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Chlorpheniramine
Applications
Antihistaminic drug
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4(pH 5.0)/CH3CN = 100/5
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Dimethindene maleate
Applications
Antihistaminic drug
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4(pH 4.6)/CH3CN = 100/9
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Promethazine
Applications
Antihistaminic drug
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4(pH 3.0)/CH3CN = 100/5
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
α-Phenylethylamine , (S)-(-)-α-Methylbenzylamine
Applications
α-Phenylethylamine
Column
ES-PhCD
Column Size
150 mm L × 6.0 mm I.D.
Mobile phase
20 mM KH2PO4(pH 4.6)/CH3CN = 95/5
Frow rate
0.6 mL/min
Column temp.
15°C

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LC

Samples
N-(3,5-Dinitrobenzoyl)-α-Methylbenzylamine
Applications
Analysis in normal phase mobile phase
Column
ES-PhCD
Column Size
150 mm L × 6.0 mm I.D.
Mobile phase
n-Hexane/C2H5OH = 85/15
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Bunitrolol
Applications
β-Blocking agent
Column
ES-PhCD
Column Size
150 mm L × 6.0 mm I.D.
Mobile phase
20 mM KH2PO4(pH 4.6)/CH3CN = 70/30
Frow rate
1.2 mL/min
Column temp.
25°C

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LC

Samples
Glucuronic acid , N-Acetylglucosamine , N-Acetylgalactosamine
Applications
Uronic acid, Acetylation amino sugar
Column
ULTRON PS-80H
Column Size
300 mm L × 8.0 mm I.D.
Mobile phase
HClO4aq.(pH 2.1)
Frow rate
1.0 mL/min
Column temp.
60°C
Pressure
2.5 MPa

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LC

Samples
Cytosine , Uracil , Guanine , Adenine , Cytidine , Uridine , Thymine , Adenosine , Guanosine , Thymidine
Applications
Nucleic acid base, Nucleoside
Column
STR ODS-II
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
0.1 M Phosphoric acid buffer(pH 2.1) + 0.2 M NaClO4
Frow rate
1.0 mL/min
Column temp.
50°C

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LC

Samples
Methylephedrine hydrochloride , Noscapine , Thiamine , Dextromethorphan , Carbinoxamine maleate
Applications
The component of the cold remedy (1)
Column
STR ODS-II
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
CH3CN/H2O/H3PO4 = 510/490/1 + 0.5% Sodium dodecyl sulfate
Frow rate
1.0 mL/min
Column temp.
50°C

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LC

Samples
Salicylic acid , Diphenhydramine , Methyl salicylate , α-Camphor , Thymol
Applications
The component of the anti-inflammatory agent
Column
STR ODS-II
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
10 mM Phosphoric acid buffer(pH 2.6) + 20 mM Heptane sodium sulphonate/CH3OH/CH3CN = 3/2/2
Frow rate
1.0 mL/min
Column temp.
45°C

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LC

Samples
Nicotinic acid , Nicotinamide , Pantothenic acid , Pyridoxine , Riboflavin phosphate , Thiamine , Caffeine , Folic acid , Biotin , Riboflavin
Applications
The water-soluble vitamin (1)
Column
STR ODS-II
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
100 mM Phosphoric acid buffer(pH 2.1) + 0.8 mM Octane sodium sulphonate/CH3CN = 9/1
Frow rate
1.0 mL/min
Column temp.
40°C

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LC

Samples
Pyridoxal , Pyridoxine , Pyridoxamine
Applications
The water-soluble vitamin (2)
Column
STR ODS-II
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
100 mM Phosphoric acid buffer(pH 2.1) + 50 mM Hexane sodium sulphonate/CH3CN = 9/1
Frow rate
1.0 mL/min
Column temp.
45°C

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LC

Samples
Nicotinic acid , Nicotinic acid amide , Calcium pantothenate , Pyridoxine hydrochloride , Riboflavin phosphate , Thiamine , Folic acid , Biotin , Riboflavin
Applications
The water-soluble vitamin
Column
VX-ODS
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM H3PO4/5 mM Sodium 1-hexanesulfonate = 91/9
Frow rate
1.0 mL/min
Column temp.
45°C

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LC

Samples
Bepotastine besilate
Applications
Bepotastine besilate
Column
ES-CD
Column Size
150 mm L × 6.0 mm I.D.
Mobile phase
20 mM KH2PO4(pH 4.6)/CH3CN = 75/25
Frow rate
0.7 mL/min
Column temp.
40°C

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LC

Samples
Bepotastine besilate
Applications
Bepotastine besilate
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4(pH 4.6)/CH3CN = 90/10
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Brompheniramine maleate
Applications
Brompheniramine maleate
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4(pH 4.6)/CH3CN = 90/10
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Bupropion hydrochloride
Applications
Bupropion hydrochloride
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4 + 20 mM K2HPO4(pH 6.0)/C2H5OH = 90/10
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Cetirizine hydrochloride
Applications
Cetirizine hydrochloride
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4 + 20 mM K2HPO4(pH 6.0)/CH3CN = 90/10
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
2 µL
Diluent
Mobile phase

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LC

Samples
Cetirizine hydrochloride
Applications
Cetirizine hydrochloride
Column
ES-OVM
Column Size
100 mm L × 3.0 mm I.D.
Mobile phase
20 mM KH2PO4 + 20 mM K2HPO4(pH 6.0)/CH3CN = 90/10
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Doxylamine succinate
Applications
Doxylamine succinate
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4 + 20 mM K2HPO4(pH 6.0)/CH3CN = 90/10
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Nicotinamide , Pyridoxine , Isoascorbic acid , Riboflavin , Nicotinic acid , Ascorbic acid , Biotin , Pantothenic acid , Folic acid , Cyanocobalamin , Thiamine
Applications
Water-soluble vitamins
Column
ULTRON AF-HILIC-CD
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
A: 20 mM CH3CO2NH4(pH 6.8)/CH3CN = 10/90, B: 20 mM CH3CO2NH4(pH 6.8)/CH3CN = 70/30
Frow rate
0.25 mL/min
Column temp.
30°C
Injection volume
1.0 µL

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LC

Samples
(CYS)2 , LYS , ARG , HIS , ASP , GLU , GLN , ASN , GLY , SER , ALA , THR , PRO , TYR , VAL , PHE , MET , TRP , LEU+ILE
Applications
Analysis of underivatized amino acids by LC/MS/MS
Column
ULTRON AF-HILIC-CD (PLSS)
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
A: 100 mM HCO2NH4(pH 3.0)/CH3CN = 10/90, B: 100 mM HCO2NH4(pH 3.0)/CH3CN = 70/30
Frow rate
0.36 mL/min
Column temp.
40°C
Injection volume
1.0 µL (5.0 µg/mL)

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LC

Samples
Fucose , Xylose , GalNAc , Mannose , Glucose , GluNAc , Galactose , Neu5Ac , Glucuronic acid
Applications
Glycan-constituting monosaccharides
Column
ULTRON AF-HILIC-CD
Column Size
150 mm L × 2.0 mm I.D.
Mobile phase
A: 200 mM CH3CO2NH4(pH 6.8)/CH3CN = 10/90 (for peak 1 to 7), B: 200 mM CH3CO2NH4(pH 6.8)/CH3CN = 18/82 (for peak 8 and 9)
Frow rate
0.26 mL/min
Column temp.
45°C
Injection volume
1.0 µL

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LC

Samples
Cyanuric acid , Ammelide , Melamine , Ammeline
Applications
Melamine-related compounds
Column
ULTRON AF-HILIC-CD
Column Size
100 mm L × 2.0 mm I.D.
Mobile phase
20 mM HCO2NH4(pH 6.8)/CH3CN = 18/82
Frow rate
0.15 mL/min
Column temp.
30°C
Injection volume
0.8 µL

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LC

Samples
L-DOPA , Dopamine , Adrenaline , Noradrenaline
Applications
Analysis of catecholamines
Column
ULTRON AF-HILIC-DA
Column Size
100 mm L × 4.6 mm I.D.
Mobile phase
20mM CH3CO2NH4 (pH4.7) /CH3CN = 10/90
Frow rate
0.50 mL/min
Column temp.
30°C
Injection volume
4.0 µL
Diluent
Mobile phase

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Graph

LC

Samples
Cyanuric acid , Ammelide , Melamine , Ammeline
Applications
Analysis of melamine compounds
Column
ULTRON AF-HILIC-CD
Column Size
100 mm L × 2.0 mm I.D.
Mobile phase
20mM HCO2NH4 (pH6.8) /CH3CN = 18/82
Frow rate
0.15 mL/min
Column temp.
30°C
Injection volume
2.0 µL
Diluent
Dissolved samples in 0.1% NaOH aq and add acetonitrile into ratio to 50%

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LC

Samples
Atomoxetine hydrochloride
Applications
Analyses of atomoxetine hydrochloride in ULTRON ES-OVM series.(Faster analyses with 3µm particles)
Column
ES-OVM
Column Size
(1)150 mm L × 4.6 mm I.D. (2)100 mm L × 3.0 mm I.D.
Mobile phase
20 mM KH2PO4 + 20 mM K2HPO4 (pH 6.0)/CH3CN = 80/20
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
(1)2.0 µL (2)0.5 µL
Diluent
methanol

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LC

Samples
Duloxetine hydrochloride
Applications
Analyses of duloxetine hydrochloride in ULTRON ES-OVM series.(Faster analyses with 3µm particles)
Column
ES-OVM
Column Size
(1)150 mm L × 4.6 mm I.D. (2)100 mm L × 3.0 mm I.D.
Mobile phase
20 mM KH2PO4 (pH 4.6)/CH3CN = 80/20
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
(1)2.0 µL (2)0.5 µL
Diluent
Mobile phase

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Graph

LC

Samples
Atomoxetine hydrochloride
Applications
Analyses of atomoxetine hydrochloride in ULTRON ES-OVM series.(Greater analytical performance with 3µm particles)
Column
ES-OVM
Column Size
(1)150 mm L × 4.6 mm I.D. (2)100 mm L × 3.0 mm I.D.
Mobile phase
20 mM KH2PO4 + 20 mM K2HPO4 (pH 6.0)/CH3CN = 80/20
Frow rate
(1)1.0 mL/min (2)0.28 mL/min
Column temp.
25°C
Injection volume
(1)2.0 µL (2)0.5 µL
Diluent
methanol

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Graph

LC

Samples
Duloxetine hydrochloride
Applications
Analyses of duloxetine hydrochloride in ULTRON ES-OVM series.(Greater analytical performance with 3µm particles)
Column
ES-OVM
Column Size
(1)150 mm L × 4.6 mm I.D. (2)100 mm L × 3.0 mm I.D.
Mobile phase
20 mM KH2PO4 (pH 4.6)/CH3CN = 80/20
Frow rate
(1)1.0 mL/min (2)0.28 mL/min
Column temp.
25°C
Injection volume
(1)2.0 µL (2)0.5 µL
Diluent
Mobile phase

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Graph

LC

Samples
Sertraline hydrochloride
Applications
Analysis of Sertraline hydrochloride
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
2.0 µL
Diluent
methanol

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Graph

LC

Samples
Sertraline hydrochloride
Applications
Analysis of Sertraline hydrochloride
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 85/15
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
2.0 µL
Diluent
methanol

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Graph

LC

Samples
Cinacalcet hydrochloride
Applications
Analysis of Cinacalcet hydrochloride
Column
ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3CN = 93/7
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
2.0 µL
Diluent
ethanol

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Graph

LC

Samples
Sertraline hydrochloride , Sertraline Hydrochloride Related Compound A
Applications
Analysis of Sertraline hydrochloride
Column
ES-CD
Column Size
250 mm L × 4.6 mm I.D.
Mobile phase
50.4mM NH4H2PO4 (pH 4.2)/CH3OH = 52/48
Frow rate
1.0 mL/min
Column temp.
30°C
Injection volume
20.0 µL
Diluent
Mobile phase

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Graph

LC

Samples
Atomoxetine hydrochloride
Applications
Analysis of atomoxetine hydrochloride
Column
ES-OVM
Column Size
100 mm L × 3.0 mm I.D.
Mobile phase
20 mM KH2PO4 + 20 mM K2HPO4 (pH 6.0)/CH3CN = 80/20
Frow rate
0.28 mL/min
Column temp.
25°C
Injection volume
0.5 µL
Diluent
methanol

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Graph

LC

Samples
Duloxetine hydrochloride
Applications
Analysis of duloxetine hydrochloride
Column
ES-OVM
Column Size
100 mm L × 3.0 mm I.D.
Mobile phase
20 mM KH2PO4 (pH 4.6)/CH3CN = 80/20
Frow rate
0.28 mL/min
Column temp.
25°C
Injection volume
0.5 µL
Diluent
Mobile phase

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